Synthesis of hexagonal boron carbonitride phase by solvothermal method

Fu Lin Huang; Chuan Bao Cao; Xu Xiang; Rui Tao Lv; He Sun Zhu

doi:10.1016/j.diamond.2004.03.001

Synthesis of hexagonal boron carbonitride phase by solvothermal method

Fu Lin Huang
, Chuan Bao Cao^*
, Xu Xiang
, Rui Tao Lv
, He Sun Zhu

^*此作品的通讯作者

材料学院

Beijing Institute of Technology

科研成果: 期刊稿件 › 文章 › 同行评审

60 引用（Scopus）

摘要

A solvothermal reaction of CH₃CN·BCl₃ and lithium nitride (Li₃N) using benzene as the solvent has been successfully applied to prepare boron carbonitride at 300°C and less than about 7 MPa. X-ray photoelectron spectroscopy (XPS) and Fourier transform infrared spectroscopy (FTIR) are used to confirm their chemical composition and atomic-level hybrid. X-ray diffraction (XRD) and transmission electron diffraction (TED) analysis indicate that the powders have hexagonal network structures.

源语言	英语
页（从-至）	1757-1760
页数	4
期刊	Diamond and Related Materials
卷	13
期	10
DOI	https://doi.org/10.1016/j.diamond.2004.03.001
出版状态	已出版 - 10月 2004

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10.1016/j.diamond.2004.03.001

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@article{e4acc31a181e4e2790d43272961b0672,

title = "Synthesis of hexagonal boron carbonitride phase by solvothermal method",

abstract = "A solvothermal reaction of CH3CN·BCl3 and lithium nitride (Li3N) using benzene as the solvent has been successfully applied to prepare boron carbonitride at 300°C and less than about 7 MPa. X-ray photoelectron spectroscopy (XPS) and Fourier transform infrared spectroscopy (FTIR) are used to confirm their chemical composition and atomic-level hybrid. X-ray diffraction (XRD) and transmission electron diffraction (TED) analysis indicate that the powders have hexagonal network structures.",

keywords = "BCN, High pressure crystal growth, Metastable phases, Solvothermal synthesis",

author = "Huang, \{Fu Lin\} and Cao, \{Chuan Bao\} and Xu Xiang and Lv, \{Rui Tao\} and Zhu, \{He Sun\}",

year = "2004",

month = oct,

doi = "10.1016/j.diamond.2004.03.001",

language = "English",

volume = "13",

pages = "1757--1760",

journal = "Diamond and Related Materials",

issn = "0925-9635",

publisher = "Elsevier B.V.",

number = "10",

}

TY - JOUR

T1 - Synthesis of hexagonal boron carbonitride phase by solvothermal method

AU - Huang, Fu Lin

AU - Cao, Chuan Bao

AU - Xiang, Xu

AU - Lv, Rui Tao

AU - Zhu, He Sun

PY - 2004/10

Y1 - 2004/10

N2 - A solvothermal reaction of CH3CN·BCl3 and lithium nitride (Li3N) using benzene as the solvent has been successfully applied to prepare boron carbonitride at 300°C and less than about 7 MPa. X-ray photoelectron spectroscopy (XPS) and Fourier transform infrared spectroscopy (FTIR) are used to confirm their chemical composition and atomic-level hybrid. X-ray diffraction (XRD) and transmission electron diffraction (TED) analysis indicate that the powders have hexagonal network structures.

AB - A solvothermal reaction of CH3CN·BCl3 and lithium nitride (Li3N) using benzene as the solvent has been successfully applied to prepare boron carbonitride at 300°C and less than about 7 MPa. X-ray photoelectron spectroscopy (XPS) and Fourier transform infrared spectroscopy (FTIR) are used to confirm their chemical composition and atomic-level hybrid. X-ray diffraction (XRD) and transmission electron diffraction (TED) analysis indicate that the powders have hexagonal network structures.

KW - BCN

KW - High pressure crystal growth

KW - Metastable phases

KW - Solvothermal synthesis

UR - https://www.scopus.com/pages/publications/9644290870

U2 - 10.1016/j.diamond.2004.03.001

DO - 10.1016/j.diamond.2004.03.001

M3 - Article

AN - SCOPUS:9644290870

SN - 0925-9635

VL - 13

SP - 1757

EP - 1760

JO - Diamond and Related Materials

JF - Diamond and Related Materials

IS - 10

ER -

Synthesis of hexagonal boron carbonitride phase by solvothermal method

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