Synthesis and characterization of a new double-cubane Mo-Fe-S cluster compound, [NEt4]3[Mo2Fe6S 8(μ-OMe)3(SPh)3Cl3]

Ji Qing Xu; Xun Gao Zhang; Hui Cai; Ning Hai Hu; Hang Ping Wei; Guo Yu Yang; Tie Gang Wang

doi:10.1039/CC9960000757

Synthesis and characterization of a new double-cubane Mo-Fe-S cluster compound, [NEt₄]₃[Mo₂Fe₆S ₈(μ-OMe)₃(SPh)₃Cl₃]

Ji Qing Xu^*
, Xun Gao Zhang
, Hui Cai
, Ning Hai Hu
, Hang Ping Wei
, Guo Yu Yang
, Tie Gang Wang

^*此作品的通讯作者

Jilin University
CAS - Changchun Institute of Applied Chemistry

科研成果: 期刊稿件 › 文章 › 同行评审

4 引用（Scopus）

摘要

The new double-cubane cluster compound [NEt₄]₃[Mo₂Fe₆S ₈(μ-OMe)₃(SPh)₃Cl₃] is synthesized from (NH₄)₂MoS₄, FeCl₃, Fe powder, S powder, NaSPh and NEt₄Br in MeOH-DMF, its crystal structure is determined by X-ray crystallography, and results of XPS indicate a valence state of +4 for Mo.

源语言	英语
页（从-至）	757-758
页数	2
期刊	Chemical Communications
期	6
DOI	https://doi.org/10.1039/CC9960000757
出版状态	已出版 - 1996
已对外发布	是

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10.1039/CC9960000757

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@article{0427683a97074b8d9cfef9551377923c,

title = "Synthesis and characterization of a new double-cubane Mo-Fe-S cluster compound, [NEt4]3[Mo2Fe6S 8(μ-OMe)3(SPh)3Cl3]",

abstract = "The new double-cubane cluster compound [NEt4]3[Mo2Fe6S 8(μ-OMe)3(SPh)3Cl3] is synthesized from (NH4)2MoS4, FeCl3, Fe powder, S powder, NaSPh and NEt4Br in MeOH-DMF, its crystal structure is determined by X-ray crystallography, and results of XPS indicate a valence state of +4 for Mo.",

author = "Xu, \{Ji Qing\} and Zhang, \{Xun Gao\} and Hui Cai and Hu, \{Ning Hai\} and Wei, \{Hang Ping\} and Yang, \{Guo Yu\} and Wang, \{Tie Gang\}",

year = "1996",

doi = "10.1039/CC9960000757",

language = "English",

pages = "757--758",

journal = "Chemical Communications",

issn = "1359-7345",

publisher = "Royal Society of Chemistry",

number = "6",

}

TY - JOUR

T1 - Synthesis and characterization of a new double-cubane Mo-Fe-S cluster compound, [NEt4]3[Mo2Fe6S 8(μ-OMe)3(SPh)3Cl3]

AU - Xu, Ji Qing

AU - Zhang, Xun Gao

AU - Cai, Hui

AU - Hu, Ning Hai

AU - Wei, Hang Ping

AU - Yang, Guo Yu

AU - Wang, Tie Gang

PY - 1996

Y1 - 1996

N2 - The new double-cubane cluster compound [NEt4]3[Mo2Fe6S 8(μ-OMe)3(SPh)3Cl3] is synthesized from (NH4)2MoS4, FeCl3, Fe powder, S powder, NaSPh and NEt4Br in MeOH-DMF, its crystal structure is determined by X-ray crystallography, and results of XPS indicate a valence state of +4 for Mo.

AB - The new double-cubane cluster compound [NEt4]3[Mo2Fe6S 8(μ-OMe)3(SPh)3Cl3] is synthesized from (NH4)2MoS4, FeCl3, Fe powder, S powder, NaSPh and NEt4Br in MeOH-DMF, its crystal structure is determined by X-ray crystallography, and results of XPS indicate a valence state of +4 for Mo.

UR - https://www.scopus.com/pages/publications/0041091212

U2 - 10.1039/CC9960000757

DO - 10.1039/CC9960000757

M3 - Article

AN - SCOPUS:0041091212

SN - 1359-7345

SP - 757

EP - 758

JO - Chemical Communications

JF - Chemical Communications

IS - 6

ER -

Synthesis and characterization of a new double-cubane Mo-Fe-S cluster compound, [NEt4]3[Mo2Fe6S 8(μ-OMe)3(SPh)3Cl3]

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Synthesis and characterization of a new double-cubane Mo-Fe-S cluster compound, [NEt₄]₃[Mo₂Fe₆S ₈(μ-OMe)₃(SPh)₃Cl₃]