TY - JOUR
T1 - Study on the Static and Dynamic Tensile Behavior of Epoxy Composites Reinforced with Nano-Alumina
AU - Zhang, Liwei
AU - Qiao, Jinchao
AU - Li, Jinzhu
N1 - Publisher Copyright:
© 2026 by the authors.
PY - 2026/8
Y1 - 2026/8
N2 - Epoxy resins suffer from inherent brittleness, limiting their reliability in impact-resistant structures. This study addresses the dispersion–performance trade-off in nano-alumina (Al2O3)/epoxy composites by fabricating specimens with 0–15 wt% filler loadings using an optimized ultrasonic-mechanical dispersion strategy. Quasi-static and dynamic tensile behaviors (600–1600 s−1) were evaluated using a universal tester and a split Hopkinson tensile bar (SHTB) system equipped with high-sensitivity semiconductor strain gauges. Results identify a critical agglomeration threshold at 3 wt%. The 1 wt% composite exhibited optimal quasi-static strength (44.76 ± 0.25 MPa), a 4.0% improvement over the neat epoxy (43.04 ± 0.33 MPa). While all composites showed positive strain-rate sensitivity, nano-Al2O3 incorporation generally reduced dynamic strength, except for the 5 wt% composite at intermediate rates. Notably, the 15 wt% composite recovered to 78.49 ± 0.48 MPa at 1600 s−1 due to high-rate energy dissipation mechanisms. Microstructural analysis revealed a transition from brittle cleavage to a hybrid fracture mode dominated by microvoids and localized plastic tearing. This work quantitatively defines the optimal loading window for nano-Al2O3/epoxy composites in protective engineering.
AB - Epoxy resins suffer from inherent brittleness, limiting their reliability in impact-resistant structures. This study addresses the dispersion–performance trade-off in nano-alumina (Al2O3)/epoxy composites by fabricating specimens with 0–15 wt% filler loadings using an optimized ultrasonic-mechanical dispersion strategy. Quasi-static and dynamic tensile behaviors (600–1600 s−1) were evaluated using a universal tester and a split Hopkinson tensile bar (SHTB) system equipped with high-sensitivity semiconductor strain gauges. Results identify a critical agglomeration threshold at 3 wt%. The 1 wt% composite exhibited optimal quasi-static strength (44.76 ± 0.25 MPa), a 4.0% improvement over the neat epoxy (43.04 ± 0.33 MPa). While all composites showed positive strain-rate sensitivity, nano-Al2O3 incorporation generally reduced dynamic strength, except for the 5 wt% composite at intermediate rates. Notably, the 15 wt% composite recovered to 78.49 ± 0.48 MPa at 1600 s−1 due to high-rate energy dissipation mechanisms. Microstructural analysis revealed a transition from brittle cleavage to a hybrid fracture mode dominated by microvoids and localized plastic tearing. This work quantitatively defines the optimal loading window for nano-Al2O3/epoxy composites in protective engineering.
KW - dynamic tensile behavior
KW - fracture toughness
KW - interfacial adhesion
KW - nano-AlO/epoxy composites
KW - particle agglomeration
KW - quasi-static tensile behavior
KW - strain rate sensitivity
UR - https://www.scopus.com/pages/publications/105047004768
U2 - 10.3390/polym18151861
DO - 10.3390/polym18151861
M3 - Article
AN - SCOPUS:105047004768
SN - 2073-4360
VL - 18
JO - Polymers
JF - Polymers
IS - 15
M1 - 1861
ER -