Preparation and molecular structure of CHZNTO·H2O

Chang Gen Feng; Li Yang; Jian Guo Zhang; Tong Lai Zhang; Kai Bei Yu

Preparation and molecular structure of CHZNTO·H₂O

Chang Gen Feng^*
, Li Yang
, Jian Guo Zhang
, Tong Lai Zhang
, Kai Bei Yu

^*此作品的通讯作者

机电学院

Beijing Institute of Technology
Chinese Academy of Sciences

科研成果: 期刊稿件 › 文章 › 同行评审

13 引用（Scopus）

摘要

CHZNTO·H₂O was prepared by mixing carbohydrazide(CHZ) and 3-nitro-1, 2, 4-triazol-5-one (NTO). The product was characterized by elemental analysis and IR measurement. The crystal structure was determined by single-crystal diffraction analysis. The crystal belongs to triclinic, space group P1 with a = 6.639(1), b = 11.481(1), c = 13.692(2) Å, a = 70.56(1), β = 88.19(1), γ = 77.03 (1)°, V = 958(2)Å³, Z = 4, D_c = 1.651 g/cm³, μ(MoKα) = 0.150 mm ^-1. F(000) = 496, R = 0.0315 and wR = 0.0894. It is concluded that CHZNTO is an ionic compound composed of one CHZ cation and one NTO anion according to the crystal structure.

源语言	英语
页（从-至）	309-312
页数	4
期刊	Jiegou Huaxue
卷	21
期	3
出版状态	已出版 - 2002

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引用此

@article{94cd3ecb1f4f48f3b7dc40f11862e200,

title = "Preparation and molecular structure of CHZNTO·H2O",

abstract = "CHZNTO·H2O was prepared by mixing carbohydrazide(CHZ) and 3-nitro-1, 2, 4-triazol-5-one (NTO). The product was characterized by elemental analysis and IR measurement. The crystal structure was determined by single-crystal diffraction analysis. The crystal belongs to triclinic, space group P1 with a = 6.639(1), b = 11.481(1), c = 13.692(2) {\AA}, a = 70.56(1), β = 88.19(1), γ = 77.03 (1)°, V = 958(2){\AA}3, Z = 4, Dc = 1.651 g/cm3, μ(MoKα) = 0.150 mm -1. F(000) = 496, R = 0.0315 and wR = 0.0894. It is concluded that CHZNTO is an ionic compound composed of one CHZ cation and one NTO anion according to the crystal structure.",

keywords = "2,4-trinzol-5-one, 3-nitro-1, Carbohydrazide, Crystal structure, Preparation",

author = "Feng, \{Chang Gen\} and Li Yang and Zhang, \{Jian Guo\} and Zhang, \{Tong Lai\} and Yu, \{Kai Bei\}",

year = "2002",

language = "English",

volume = "21",

pages = "309--312",

journal = "Jiegou Huaxue",

issn = "0254-5861",

publisher = "Fujian Institute of Research of the Structure of Matter",

number = "3",

}

TY - JOUR

T1 - Preparation and molecular structure of CHZNTO·H2O

AU - Feng, Chang Gen

AU - Yang, Li

AU - Zhang, Jian Guo

AU - Zhang, Tong Lai

AU - Yu, Kai Bei

PY - 2002

Y1 - 2002

N2 - CHZNTO·H2O was prepared by mixing carbohydrazide(CHZ) and 3-nitro-1, 2, 4-triazol-5-one (NTO). The product was characterized by elemental analysis and IR measurement. The crystal structure was determined by single-crystal diffraction analysis. The crystal belongs to triclinic, space group P1 with a = 6.639(1), b = 11.481(1), c = 13.692(2) Å, a = 70.56(1), β = 88.19(1), γ = 77.03 (1)°, V = 958(2)Å3, Z = 4, Dc = 1.651 g/cm3, μ(MoKα) = 0.150 mm -1. F(000) = 496, R = 0.0315 and wR = 0.0894. It is concluded that CHZNTO is an ionic compound composed of one CHZ cation and one NTO anion according to the crystal structure.

AB - CHZNTO·H2O was prepared by mixing carbohydrazide(CHZ) and 3-nitro-1, 2, 4-triazol-5-one (NTO). The product was characterized by elemental analysis and IR measurement. The crystal structure was determined by single-crystal diffraction analysis. The crystal belongs to triclinic, space group P1 with a = 6.639(1), b = 11.481(1), c = 13.692(2) Å, a = 70.56(1), β = 88.19(1), γ = 77.03 (1)°, V = 958(2)Å3, Z = 4, Dc = 1.651 g/cm3, μ(MoKα) = 0.150 mm -1. F(000) = 496, R = 0.0315 and wR = 0.0894. It is concluded that CHZNTO is an ionic compound composed of one CHZ cation and one NTO anion according to the crystal structure.

KW - 2,4-trinzol-5-one

KW - 3-nitro-1

KW - Carbohydrazide

KW - Crystal structure

KW - Preparation

UR - https://www.scopus.com/pages/publications/33845336550

M3 - Article

AN - SCOPUS:33845336550

SN - 0254-5861

VL - 21

SP - 309

EP - 312

JO - Jiegou Huaxue

JF - Jiegou Huaxue

IS - 3

ER -

Preparation and molecular structure of CHZNTO·H2O

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Preparation and molecular structure of CHZNTO·H₂O