Preparation and evaluation of serine derivatived β-cyclodextrin column for high performance liquid chromatography

Li Na Geng; Yan Li; Yu Pang; Shuang Yu; Li Quan Sun; Ai Qin Luo

Preparation and evaluation of serine derivatived β-cyclodextrin column for high performance liquid chromatography

Li Na Geng^*
, Yan Li
, Yu Pang
, Shuang Yu
, Li Quan Sun
, Ai Qin Luo

^*此作品的通讯作者

生命学院

Beijing Institute of Technology

科研成果: 期刊稿件 › 文章 › 同行评审

摘要

Chromatography column packing of the newly prepared carbobenzyloxy-L-Ser derived β-CD bonded phase (SCDS), along with the underived β-CD bonded phase (CDS) were investigated. Satisfactory column efficiency, peak shape and reproducibility were obtained by optimizing high pressure column packing technology, such as packing pressure and slurry dispersing medium. The separation performance of SCDS for several position isomers and chiral compounds were also investigated and compared with CDS. The newly prepared column exhibited specific properties in realizing isomers separation.

源语言	英语
页（从-至）	1022-1026
页数	5
期刊	Beijing Ligong Daxue Xuebao/Transaction of Beijing Institute of Technology
卷	27
期	11
出版状态	已出版 - 11月 2007

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title = "Preparation and evaluation of serine derivatived β-cyclodextrin column for high performance liquid chromatography",

abstract = "Chromatography column packing of the newly prepared carbobenzyloxy-L-Ser derived β-CD bonded phase (SCDS), along with the underived β-CD bonded phase (CDS) were investigated. Satisfactory column efficiency, peak shape and reproducibility were obtained by optimizing high pressure column packing technology, such as packing pressure and slurry dispersing medium. The separation performance of SCDS for several position isomers and chiral compounds were also investigated and compared with CDS. The newly prepared column exhibited specific properties in realizing isomers separation.",

keywords = "Column packing technology, High performance liquid chromatography, Isomer separation, Serine derivatived β-cyclodextrin",

author = "Geng, \{Li Na\} and Yan Li and Yu Pang and Shuang Yu and Sun, \{Li Quan\} and Luo, \{Ai Qin\}",

year = "2007",

month = nov,

language = "English",

volume = "27",

pages = "1022--1026",

journal = "Beijing Ligong Daxue Xuebao/Transaction of Beijing Institute of Technology",

issn = "1001-0645",

publisher = "Beijing Institute of Technology",

number = "11",

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TY - JOUR

T1 - Preparation and evaluation of serine derivatived β-cyclodextrin column for high performance liquid chromatography

AU - Geng, Li Na

AU - Li, Yan

AU - Pang, Yu

AU - Yu, Shuang

AU - Sun, Li Quan

AU - Luo, Ai Qin

PY - 2007/11

Y1 - 2007/11

N2 - Chromatography column packing of the newly prepared carbobenzyloxy-L-Ser derived β-CD bonded phase (SCDS), along with the underived β-CD bonded phase (CDS) were investigated. Satisfactory column efficiency, peak shape and reproducibility were obtained by optimizing high pressure column packing technology, such as packing pressure and slurry dispersing medium. The separation performance of SCDS for several position isomers and chiral compounds were also investigated and compared with CDS. The newly prepared column exhibited specific properties in realizing isomers separation.

AB - Chromatography column packing of the newly prepared carbobenzyloxy-L-Ser derived β-CD bonded phase (SCDS), along with the underived β-CD bonded phase (CDS) were investigated. Satisfactory column efficiency, peak shape and reproducibility were obtained by optimizing high pressure column packing technology, such as packing pressure and slurry dispersing medium. The separation performance of SCDS for several position isomers and chiral compounds were also investigated and compared with CDS. The newly prepared column exhibited specific properties in realizing isomers separation.

KW - Column packing technology

KW - High performance liquid chromatography

KW - Isomer separation

KW - Serine derivatived β-cyclodextrin

UR - https://www.scopus.com/pages/publications/37349122448

M3 - Article

AN - SCOPUS:37349122448

SN - 1001-0645

VL - 27

SP - 1022

EP - 1026

JO - Beijing Ligong Daxue Xuebao/Transaction of Beijing Institute of Technology

JF - Beijing Ligong Daxue Xuebao/Transaction of Beijing Institute of Technology

IS - 11

ER -

Preparation and evaluation of serine derivatived β-cyclodextrin column for high performance liquid chromatography

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