Polyol mediated synthesis of nanocrystalline M3SbS3 (M = Ag, Cu)

Di Chen; Guozhen Shen; Kaibin Tang; Xuan Jiang; Liying Huang; Yin Jin; Yitai Qian

doi:10.1016/S0025-5408(02)01054-1

Polyol mediated synthesis of nanocrystalline M₃SbS₃ (M = Ag, Cu)

Di Chen
, Guozhen Shen
, Kaibin Tang
, Xuan Jiang
, Liying Huang
, Yin Jin
, Yitai Qian

University of Science and Technology of China

科研成果: 期刊稿件 › 文章 › 同行评审

15 引用（Scopus）

摘要

A simple and convenient polyol-mediated route has been developed to produce nanocrystalline Ag₃SbS₃ and Cu₃SbS₃ from AgNO₃ and Cu(NO₃)₂ and SbCl₃ with thiourea at 197°C. The products were characterized by X-ray powder diffraction, X-ray photoelectron spectroscopy, and transmission electron microscopy. Analysis shows that glycol agitated state and injection rate have a great effect on the purity of the final products.

源语言	英语
页（从-至）	509-513
页数	5
期刊	Materials Research Bulletin
卷	38
期	3
DOI	https://doi.org/10.1016/S0025-5408(02)01054-1
出版状态	已出版 - 20 2月 2003
已对外发布	是

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10.1016/S0025-5408(02)01054-1

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title = "Polyol mediated synthesis of nanocrystalline M3SbS3 (M = Ag, Cu)",

abstract = "A simple and convenient polyol-mediated route has been developed to produce nanocrystalline Ag3SbS3 and Cu3SbS3 from AgNO3 and Cu(NO3)2 and SbCl3 with thiourea at 197°C. The products were characterized by X-ray powder diffraction, X-ray photoelectron spectroscopy, and transmission electron microscopy. Analysis shows that glycol agitated state and injection rate have a great effect on the purity of the final products.",

keywords = "Chemical synthesis, Electron microscopy, Nanostructures",

author = "Di Chen and Guozhen Shen and Kaibin Tang and Xuan Jiang and Liying Huang and Yin Jin and Yitai Qian",

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T1 - Polyol mediated synthesis of nanocrystalline M3SbS3 (M = Ag, Cu)

AU - Chen, Di

AU - Shen, Guozhen

AU - Tang, Kaibin

AU - Jiang, Xuan

AU - Huang, Liying

AU - Jin, Yin

AU - Qian, Yitai

PY - 2003/2/20

Y1 - 2003/2/20

N2 - A simple and convenient polyol-mediated route has been developed to produce nanocrystalline Ag3SbS3 and Cu3SbS3 from AgNO3 and Cu(NO3)2 and SbCl3 with thiourea at 197°C. The products were characterized by X-ray powder diffraction, X-ray photoelectron spectroscopy, and transmission electron microscopy. Analysis shows that glycol agitated state and injection rate have a great effect on the purity of the final products.

AB - A simple and convenient polyol-mediated route has been developed to produce nanocrystalline Ag3SbS3 and Cu3SbS3 from AgNO3 and Cu(NO3)2 and SbCl3 with thiourea at 197°C. The products were characterized by X-ray powder diffraction, X-ray photoelectron spectroscopy, and transmission electron microscopy. Analysis shows that glycol agitated state and injection rate have a great effect on the purity of the final products.

KW - Chemical synthesis

KW - Electron microscopy

KW - Nanostructures

UR - https://www.scopus.com/pages/publications/0037456511

U2 - 10.1016/S0025-5408(02)01054-1

DO - 10.1016/S0025-5408(02)01054-1

M3 - Article

AN - SCOPUS:0037456511

SN - 0025-5408

VL - 38

SP - 509

EP - 513

JO - Materials Research Bulletin

JF - Materials Research Bulletin

IS - 3

ER -

Polyol mediated synthesis of nanocrystalline M3SbS3 (M = Ag, Cu)

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Polyol mediated synthesis of nanocrystalline M₃SbS₃ (M = Ag, Cu)