Influence of Fe-doping on the structural, optical and magnetic properties of ZnO nanoparticles

Changzhen Liu; Dawei Meng; Haixia Pang; Xiuling Wu; Jing Xie; Xiaohong Yu; Long Chen; Xiaoyang Liu

doi:10.1016/j.jmmm.2012.05.054

Influence of Fe-doping on the structural, optical and magnetic properties of ZnO nanoparticles

Changzhen Liu
, Dawei Meng^*
, Haixia Pang
, Xiuling Wu
, Jing Xie
, Xiaohong Yu
, Long Chen
, Xiaoyang Liu

^*此作品的通讯作者

China University of Geosciences, Wuhan
Jilin University
Hubei University of Technology

科研成果: 期刊稿件 › 文章 › 同行评审

87 引用（Scopus）

摘要

Zn _1-xFe _xO (x=0-0.05) nanoparticles were synthesized without a catalyst by a two-step method. Fe was doped into ZnO by a source of metallic Fe sheets in a solid-liquid system at 80 °C, and the Zn _1-xFe _xO nanoparticles were obtained by annealing at 300 °C. X-ray diffraction, X-ray photoelectron spectroscopy (XPS) and transmission electron microscopy were used to characterize the structural properties of the as-grown Zn _1-xFe _xO. The optical properties were determined by Infrared and Ultraviolet-visible spectroscopy. The results confirm that the crystallinity of the ZnO is deteriorated due to Fe-doping. XPS results show that there is a mixture of Fe ⁰ and the Fe ³ in the representative Zn _0.95Fe _0.05O sample. The optical band gap of Zn _1-xFe _xO is enhanced with increasing of Fe-doping. Room temperature ferromagnetism was observed in all the Fe-doped ZnO samples.

源语言	英语
页（从-至）	3356-3360
页数	5
期刊	Journal of Magnetism and Magnetic Materials
卷	324
期	20
DOI	https://doi.org/10.1016/j.jmmm.2012.05.054
出版状态	已出版 - 10月 2012
已对外发布	是

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title = "Influence of Fe-doping on the structural, optical and magnetic properties of ZnO nanoparticles",

abstract = "Zn 1-xFe xO (x=0-0.05) nanoparticles were synthesized without a catalyst by a two-step method. Fe was doped into ZnO by a source of metallic Fe sheets in a solid-liquid system at 80 °C, and the Zn 1-xFe xO nanoparticles were obtained by annealing at 300 °C. X-ray diffraction, X-ray photoelectron spectroscopy (XPS) and transmission electron microscopy were used to characterize the structural properties of the as-grown Zn 1-xFe xO. The optical properties were determined by Infrared and Ultraviolet-visible spectroscopy. The results confirm that the crystallinity of the ZnO is deteriorated due to Fe-doping. XPS results show that there is a mixture of Fe 0 and the Fe 3 in the representative Zn 0.95Fe 0.05O sample. The optical band gap of Zn 1-xFe xO is enhanced with increasing of Fe-doping. Room temperature ferromagnetism was observed in all the Fe-doped ZnO samples.",

keywords = "Fe-doping, Ferromagnetism, Optical property, Structural, ZnO",

author = "Changzhen Liu and Dawei Meng and Haixia Pang and Xiuling Wu and Jing Xie and Xiaohong Yu and Long Chen and Xiaoyang Liu",

year = "2012",

month = oct,

doi = "10.1016/j.jmmm.2012.05.054",

language = "English",

volume = "324",

pages = "3356--3360",

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TY - JOUR

T1 - Influence of Fe-doping on the structural, optical and magnetic properties of ZnO nanoparticles

AU - Liu, Changzhen

AU - Meng, Dawei

AU - Pang, Haixia

AU - Wu, Xiuling

AU - Xie, Jing

AU - Yu, Xiaohong

AU - Chen, Long

AU - Liu, Xiaoyang

PY - 2012/10

Y1 - 2012/10

N2 - Zn 1-xFe xO (x=0-0.05) nanoparticles were synthesized without a catalyst by a two-step method. Fe was doped into ZnO by a source of metallic Fe sheets in a solid-liquid system at 80 °C, and the Zn 1-xFe xO nanoparticles were obtained by annealing at 300 °C. X-ray diffraction, X-ray photoelectron spectroscopy (XPS) and transmission electron microscopy were used to characterize the structural properties of the as-grown Zn 1-xFe xO. The optical properties were determined by Infrared and Ultraviolet-visible spectroscopy. The results confirm that the crystallinity of the ZnO is deteriorated due to Fe-doping. XPS results show that there is a mixture of Fe 0 and the Fe 3 in the representative Zn 0.95Fe 0.05O sample. The optical band gap of Zn 1-xFe xO is enhanced with increasing of Fe-doping. Room temperature ferromagnetism was observed in all the Fe-doped ZnO samples.

AB - Zn 1-xFe xO (x=0-0.05) nanoparticles were synthesized without a catalyst by a two-step method. Fe was doped into ZnO by a source of metallic Fe sheets in a solid-liquid system at 80 °C, and the Zn 1-xFe xO nanoparticles were obtained by annealing at 300 °C. X-ray diffraction, X-ray photoelectron spectroscopy (XPS) and transmission electron microscopy were used to characterize the structural properties of the as-grown Zn 1-xFe xO. The optical properties were determined by Infrared and Ultraviolet-visible spectroscopy. The results confirm that the crystallinity of the ZnO is deteriorated due to Fe-doping. XPS results show that there is a mixture of Fe 0 and the Fe 3 in the representative Zn 0.95Fe 0.05O sample. The optical band gap of Zn 1-xFe xO is enhanced with increasing of Fe-doping. Room temperature ferromagnetism was observed in all the Fe-doped ZnO samples.

KW - Fe-doping

KW - Ferromagnetism

KW - Optical property

KW - Structural

KW - ZnO

UR - https://www.scopus.com/pages/publications/84863315488

U2 - 10.1016/j.jmmm.2012.05.054

DO - 10.1016/j.jmmm.2012.05.054

M3 - Article

AN - SCOPUS:84863315488

SN - 0304-8853

VL - 324

SP - 3356

EP - 3360

JO - Journal of Magnetism and Magnetic Materials

JF - Journal of Magnetism and Magnetic Materials

IS - 20

ER -

Influence of Fe-doping on the structural, optical and magnetic properties of ZnO nanoparticles

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