Crystal structure of 2-phenyl-9-hydrazino-1,10-phenanthroline

Yue Yang; Peiju Yang; Cui Zhang; Biao Wu

doi:10.2116/analscix.24.x97

Crystal structure of 2-phenyl-9-hydrazino-1,10-phenanthroline

Yue Yang^*
, Peiju Yang
, Cui Zhang
, Biao Wu

^*此作品的通讯作者

CAS - Lanzhou Institute of Chemical Physics
University of Chinese Academy of Sciences

科研成果: 期刊稿件 › 评论/辩论

2 引用（Scopus）

摘要

The title compound, 2-phenyl-9-hydrazino-1,10-phenanthroline, crystallizes in the monoclinic space group P2₁/c with the following unit-cell parameters: a = 11.7738(3)Å, b = 20.9998(6)Å, c = 12.4546(4)Å, β = 106.750(1)° and V = 2948.71(15)Å³. The crystal structure was solved with a final R = 0.0612 using 6260 independent reflections; it contains two independent molecules in an asymmetric unit, which are joined into a dimer by hydrogen bonds between a phenanthroline N atom and the NH donor of the hydrazine substituent. 2008

源语言	英语
页（从-至）	x97-x98
期刊	Analytical Sciences: X-ray Structure Analysis Online
卷	24
期	5
DOI	https://doi.org/10.2116/analscix.24.x97
出版状态	已出版 - 2008
已对外发布	是

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@article{7c408fd53e1e4bc392a9103539362231,

title = "Crystal structure of 2-phenyl-9-hydrazino-1,10-phenanthroline",

abstract = "The title compound, 2-phenyl-9-hydrazino-1,10-phenanthroline, crystallizes in the monoclinic space group P21/c with the following unit-cell parameters: a = 11.7738(3){\AA}, b = 20.9998(6){\AA}, c = 12.4546(4){\AA}, β = 106.750(1)° and V = 2948.71(15){\AA}3. The crystal structure was solved with a final R = 0.0612 using 6260 independent reflections; it contains two independent molecules in an asymmetric unit, which are joined into a dimer by hydrogen bonds between a phenanthroline N atom and the NH donor of the hydrazine substituent. 2008",

author = "Yue Yang and Peiju Yang and Cui Zhang and Biao Wu",

year = "2008",

doi = "10.2116/analscix.24.x97",

language = "English",

volume = "24",

pages = "x97--x98",

journal = "Analytical Sciences: X-ray Structure Analysis Online",

issn = "1348-2238",

publisher = "Japan Society for Analytical Chemistry",

number = "5",

}

TY - JOUR

T1 - Crystal structure of 2-phenyl-9-hydrazino-1,10-phenanthroline

AU - Yang, Yue

AU - Yang, Peiju

AU - Zhang, Cui

AU - Wu, Biao

PY - 2008

Y1 - 2008

N2 - The title compound, 2-phenyl-9-hydrazino-1,10-phenanthroline, crystallizes in the monoclinic space group P21/c with the following unit-cell parameters: a = 11.7738(3)Å, b = 20.9998(6)Å, c = 12.4546(4)Å, β = 106.750(1)° and V = 2948.71(15)Å3. The crystal structure was solved with a final R = 0.0612 using 6260 independent reflections; it contains two independent molecules in an asymmetric unit, which are joined into a dimer by hydrogen bonds between a phenanthroline N atom and the NH donor of the hydrazine substituent. 2008

AB - The title compound, 2-phenyl-9-hydrazino-1,10-phenanthroline, crystallizes in the monoclinic space group P21/c with the following unit-cell parameters: a = 11.7738(3)Å, b = 20.9998(6)Å, c = 12.4546(4)Å, β = 106.750(1)° and V = 2948.71(15)Å3. The crystal structure was solved with a final R = 0.0612 using 6260 independent reflections; it contains two independent molecules in an asymmetric unit, which are joined into a dimer by hydrogen bonds between a phenanthroline N atom and the NH donor of the hydrazine substituent. 2008

UR - https://www.scopus.com/pages/publications/58149473773

U2 - 10.2116/analscix.24.x97

DO - 10.2116/analscix.24.x97

M3 - Comment/debate

AN - SCOPUS:58149473773

SN - 1348-2238

VL - 24

SP - x97-x98

JO - Analytical Sciences: X-ray Structure Analysis Online

JF - Analytical Sciences: X-ray Structure Analysis Online

IS - 5

ER -

Crystal structure of 2-phenyl-9-hydrazino-1,10-phenanthroline

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