Template-assisted synthesis of Sb8O10(OH)2I2 tubular crystals under hydrothermal conditions

Qing Yang; Kaibin Tang; Chunrui Wang; Fuping Li; Bin Hai; Guozhen Shen; Changhua An; Weichao Yu; Yitai Qian

doi:10.1016/S0022-0248(01)01504-4

Template-assisted synthesis of Sb₈O₁₀(OH)₂I₂ tubular crystals under hydrothermal conditions

Qing Yang
, Kaibin Tang^*
, Chunrui Wang
, Fuping Li
, Bin Hai
, Guozhen Shen
, Changhua An
, Weichao Yu
, Yitai Qian

^*Corresponding author for this work

University of Science and Technology of China

Research output: Contribution to journal › Article › peer-review

5 Citations (Scopus)

Abstract

Mesoscale octaantimony decaoxide dihydroxide iodide (Sb₈O₁₀(OH)₂I₂) tubular crystals have been successfully synthesized for the first time through a hydrothermal route from Sb₂S₃, NaI and NaOH at 200°C. In the process, the Sb₂S₃ prismatic crystals serve as templates and play an important role in the formation of the Sb₈O₁₀(OH)₂I₂ tubular crystals in alkali aqueous solution. The products are characterized by X-ray powder diffraction and scanning electron microscopy. The sample has tubular prismatic structure. A typical tubule is 6-8mm in length, 30-50μm in diameter, and 5μm in thickness.

Original language	English
Pages (from-to)	287-291
Number of pages	5
Journal	Journal of Crystal Growth
Volume	233
Issue number	1-2
DOIs	https://doi.org/10.1016/S0022-0248(01)01504-4
Publication status	Published - Nov 2001
Externally published	Yes

Keywords

A1. X-ray diffraction
A2. hydrothermal crystal growth
B1. inorganic compounds

Access to Document

10.1016/S0022-0248(01)01504-4

Cite this

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title = "Template-assisted synthesis of Sb8O10(OH)2I2 tubular crystals under hydrothermal conditions",

abstract = "Mesoscale octaantimony decaoxide dihydroxide iodide (Sb8O10(OH)2I2) tubular crystals have been successfully synthesized for the first time through a hydrothermal route from Sb2S3, NaI and NaOH at 200°C. In the process, the Sb2S3 prismatic crystals serve as templates and play an important role in the formation of the Sb8O10(OH)2I2 tubular crystals in alkali aqueous solution. The products are characterized by X-ray powder diffraction and scanning electron microscopy. The sample has tubular prismatic structure. A typical tubule is 6-8mm in length, 30-50μm in diameter, and 5μm in thickness.",

keywords = "A1. X-ray diffraction, A2. hydrothermal crystal growth, B1. inorganic compounds",

author = "Qing Yang and Kaibin Tang and Chunrui Wang and Fuping Li and Bin Hai and Guozhen Shen and Changhua An and Weichao Yu and Yitai Qian",

year = "2001",

month = nov,

doi = "10.1016/S0022-0248(01)01504-4",

language = "English",

volume = "233",

pages = "287--291",

journal = "Journal of Crystal Growth",

issn = "0022-0248",

publisher = "Elsevier B.V.",

number = "1-2",

}

TY - JOUR

T1 - Template-assisted synthesis of Sb8O10(OH)2I2 tubular crystals under hydrothermal conditions

AU - Yang, Qing

AU - Tang, Kaibin

AU - Wang, Chunrui

AU - Li, Fuping

AU - Hai, Bin

AU - Shen, Guozhen

AU - An, Changhua

AU - Yu, Weichao

AU - Qian, Yitai

PY - 2001/11

Y1 - 2001/11

N2 - Mesoscale octaantimony decaoxide dihydroxide iodide (Sb8O10(OH)2I2) tubular crystals have been successfully synthesized for the first time through a hydrothermal route from Sb2S3, NaI and NaOH at 200°C. In the process, the Sb2S3 prismatic crystals serve as templates and play an important role in the formation of the Sb8O10(OH)2I2 tubular crystals in alkali aqueous solution. The products are characterized by X-ray powder diffraction and scanning electron microscopy. The sample has tubular prismatic structure. A typical tubule is 6-8mm in length, 30-50μm in diameter, and 5μm in thickness.

AB - Mesoscale octaantimony decaoxide dihydroxide iodide (Sb8O10(OH)2I2) tubular crystals have been successfully synthesized for the first time through a hydrothermal route from Sb2S3, NaI and NaOH at 200°C. In the process, the Sb2S3 prismatic crystals serve as templates and play an important role in the formation of the Sb8O10(OH)2I2 tubular crystals in alkali aqueous solution. The products are characterized by X-ray powder diffraction and scanning electron microscopy. The sample has tubular prismatic structure. A typical tubule is 6-8mm in length, 30-50μm in diameter, and 5μm in thickness.

KW - A1. X-ray diffraction

KW - A2. hydrothermal crystal growth

KW - B1. inorganic compounds

UR - https://www.scopus.com/pages/publications/0035501993

U2 - 10.1016/S0022-0248(01)01504-4

DO - 10.1016/S0022-0248(01)01504-4

M3 - Article

AN - SCOPUS:0035501993

SN - 0022-0248

VL - 233

SP - 287

EP - 291

JO - Journal of Crystal Growth

JF - Journal of Crystal Growth

IS - 1-2

ER -

Template-assisted synthesis of Sb₈O₁₀(OH)₂I₂ tubular crystals under hydrothermal conditions

Abstract

Keywords

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