Sythesis of the mesoporous molecular sieve MCM-41 and 129Xe NMR studies

Ke Ning Sun; Ying Cao; Yan Bin Shao

Sythesis of the mesoporous molecular sieve MCM-41 and ¹²⁹Xe NMR studies

Ke Ning Sun^*, Ying Cao, Yan Bin Shao

^*Corresponding author for this work

Harbin Institute of Technology

Research output: Contribution to journal › Article › peer-review

Abstract

Purely siliceous MCM-41 with a narrow pore - size distribution , different pore size , high surface area was synthesized . As prepared , calcined and catalytically tested MCM-41 materials have been comprehensively characterized by N₂ adsorption/desorption at 77K and ¹²⁹Xe NMR . By adding mesitylene during the synthesis , the pore size of MCM-41 was enlarged to 5. 2nm. The chemical shift in ¹²⁹Xe NMR spectroscopy of adsorbed xenon indicates that the MCM-41 is one-dimensional pore channels.

Original language	English
Pages (from-to)	118
Number of pages	1
Journal	Chinese Journal of Inorganic Chemistry
Volume	16
Issue number	1
Publication status	Published - Jan 2000
Externally published	Yes

Keywords

MCM-41 mesporous material
Xe NMR

Cite this

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title = "Sythesis of the mesoporous molecular sieve MCM-41 and 129Xe NMR studies",

abstract = "Purely siliceous MCM-41 with a narrow pore - size distribution , different pore size , high surface area was synthesized . As prepared , calcined and catalytically tested MCM-41 materials have been comprehensively characterized by N2 adsorption/desorption at 77K and 129Xe NMR . By adding mesitylene during the synthesis , the pore size of MCM-41 was enlarged to 5. 2nm. The chemical shift in 129Xe NMR spectroscopy of adsorbed xenon indicates that the MCM-41 is one-dimensional pore channels.",

keywords = "MCM-41 mesporous material, Xe NMR",

author = "Sun, \{Ke Ning\} and Ying Cao and Shao, \{Yan Bin\}",

year = "2000",

month = jan,

language = "English",

volume = "16",

pages = "118",

journal = "Chinese Journal of Inorganic Chemistry",

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T1 - Sythesis of the mesoporous molecular sieve MCM-41 and 129Xe NMR studies

AU - Sun, Ke Ning

AU - Cao, Ying

AU - Shao, Yan Bin

PY - 2000/1

Y1 - 2000/1

N2 - Purely siliceous MCM-41 with a narrow pore - size distribution , different pore size , high surface area was synthesized . As prepared , calcined and catalytically tested MCM-41 materials have been comprehensively characterized by N2 adsorption/desorption at 77K and 129Xe NMR . By adding mesitylene during the synthesis , the pore size of MCM-41 was enlarged to 5. 2nm. The chemical shift in 129Xe NMR spectroscopy of adsorbed xenon indicates that the MCM-41 is one-dimensional pore channels.

AB - Purely siliceous MCM-41 with a narrow pore - size distribution , different pore size , high surface area was synthesized . As prepared , calcined and catalytically tested MCM-41 materials have been comprehensively characterized by N2 adsorption/desorption at 77K and 129Xe NMR . By adding mesitylene during the synthesis , the pore size of MCM-41 was enlarged to 5. 2nm. The chemical shift in 129Xe NMR spectroscopy of adsorbed xenon indicates that the MCM-41 is one-dimensional pore channels.

KW - MCM-41 mesporous material

KW - Xe NMR

UR - https://www.scopus.com/pages/publications/33750844832

M3 - Article

AN - SCOPUS:33750844832

SN - 1001-4861

VL - 16

SP - 118

JO - Chinese Journal of Inorganic Chemistry

JF - Chinese Journal of Inorganic Chemistry

IS - 1

ER -

Sythesis of the mesoporous molecular sieve MCM-41 and ¹²⁹Xe NMR studies

Abstract

Keywords

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