Synthesis of ZrC hollow nanospheres at low temperature

Guozhen Shen; Di Chen; Yuanfang Liu; Kaibin Tang; Yitai Qian

doi:10.1016/j.jcrysgro.2003.10.022

Synthesis of ZrC hollow nanospheres at low temperature

Guozhen Shen^*, Di Chen, Yuanfang Liu, Kaibin Tang, Yitai Qian

^*Corresponding author for this work

University of Science and Technology of China

Research output: Contribution to journal › Article › peer-review

35 Citations (Scopus)

Abstract

A novel chemical synthetic route has been developed to prepare ZrC hollow nanospheres at 600°C, using ZrCl₄ and C₆Cl ₆ as source materials, and metallic Na as the reductant. The samples were characterized by X-ray powder diffraction and transmission electron microscopy. And an in situ template reduction-carbonization mechanism for ZrC hollow nanospheres was proposed.

Original language	English
Pages (from-to)	277-280
Number of pages	4
Journal	Journal of Crystal Growth
Volume	262
Issue number	1-4
DOIs	https://doi.org/10.1016/j.jcrysgro.2003.10.022
Publication status	Published - 15 Feb 2004
Externally published	Yes

Keywords

A1. Nanostructures
A1. X-ray diffraction
B1. Nanomaterials

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10.1016/j.jcrysgro.2003.10.022

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title = "Synthesis of ZrC hollow nanospheres at low temperature",

abstract = "A novel chemical synthetic route has been developed to prepare ZrC hollow nanospheres at 600°C, using ZrCl4 and C6Cl 6 as source materials, and metallic Na as the reductant. The samples were characterized by X-ray powder diffraction and transmission electron microscopy. And an in situ template reduction-carbonization mechanism for ZrC hollow nanospheres was proposed.",

keywords = "A1. Nanostructures, A1. X-ray diffraction, B1. Nanomaterials",

author = "Guozhen Shen and Di Chen and Yuanfang Liu and Kaibin Tang and Yitai Qian",

year = "2004",

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doi = "10.1016/j.jcrysgro.2003.10.022",

language = "English",

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journal = "Journal of Crystal Growth",

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TY - JOUR

T1 - Synthesis of ZrC hollow nanospheres at low temperature

AU - Shen, Guozhen

AU - Chen, Di

AU - Liu, Yuanfang

AU - Tang, Kaibin

AU - Qian, Yitai

PY - 2004/2/15

Y1 - 2004/2/15

N2 - A novel chemical synthetic route has been developed to prepare ZrC hollow nanospheres at 600°C, using ZrCl4 and C6Cl 6 as source materials, and metallic Na as the reductant. The samples were characterized by X-ray powder diffraction and transmission electron microscopy. And an in situ template reduction-carbonization mechanism for ZrC hollow nanospheres was proposed.

AB - A novel chemical synthetic route has been developed to prepare ZrC hollow nanospheres at 600°C, using ZrCl4 and C6Cl 6 as source materials, and metallic Na as the reductant. The samples were characterized by X-ray powder diffraction and transmission electron microscopy. And an in situ template reduction-carbonization mechanism for ZrC hollow nanospheres was proposed.

KW - A1. Nanostructures

KW - A1. X-ray diffraction

KW - B1. Nanomaterials

UR - http://www.scopus.com/inward/record.url?scp=0842330014&partnerID=8YFLogxK

U2 - 10.1016/j.jcrysgro.2003.10.022

DO - 10.1016/j.jcrysgro.2003.10.022

M3 - Article

AN - SCOPUS:0842330014

SN - 0022-0248

VL - 262

SP - 277

EP - 280

JO - Journal of Crystal Growth

JF - Journal of Crystal Growth

IS - 1-4

ER -

Synthesis of ZrC hollow nanospheres at low temperature

Abstract

Keywords

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