TY - JOUR
T1 - Synthesis of Sb 2E 3 (E =5, Se) nanorods with a flat cross section by a rapid hot injection method
AU - Ye, Mingfu
AU - Li, Yunchao
AU - Zhong, Haizheng
AU - Zhou, Yi
AU - Yang, Yi
AU - Ding, Yuqin
AU - Li, Yongfang
PY - 2010/11
Y1 - 2010/11
N2 - We report herein a simple colloidal synthesis route, i.e., rapid injection of E (E = 5, Se) source into a hot solvent (1-octadecence, ODE) containing antimony precursor (antimony stearate), to grow Sb 2E 3 nanorods. The as-prepared nanorods were extensively characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), selected area electron diffraction (SAED), and high-resolution transmission electron microscopy (HRTEM). The mechanism for growth of Sb 2E 3 nanorods was also clarified from the view of crystal structure- directed growth. We believe that the method present here is a more straightforward and cost- effective route to prepare Sb 2E 3 nanocrystals with high quality.
AB - We report herein a simple colloidal synthesis route, i.e., rapid injection of E (E = 5, Se) source into a hot solvent (1-octadecence, ODE) containing antimony precursor (antimony stearate), to grow Sb 2E 3 nanorods. The as-prepared nanorods were extensively characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), selected area electron diffraction (SAED), and high-resolution transmission electron microscopy (HRTEM). The mechanism for growth of Sb 2E 3 nanorods was also clarified from the view of crystal structure- directed growth. We believe that the method present here is a more straightforward and cost- effective route to prepare Sb 2E 3 nanocrystals with high quality.
KW - Crystal growth
KW - One-dimension nanostructures
KW - Sb S nanocrystals
KW - Sb Se nanocrystals
KW - Shape-controlled synthesis
UR - http://www.scopus.com/inward/record.url?scp=78650397613&partnerID=8YFLogxK
U2 - 10.1166/jnn.2010.2871
DO - 10.1166/jnn.2010.2871
M3 - Article
AN - SCOPUS:78650397613
SN - 1533-4880
VL - 10
SP - 7778
EP - 7782
JO - Journal of Nanoscience and Nanotechnology
JF - Journal of Nanoscience and Nanotechnology
IS - 11
ER -