Abstract
Different polyimide oligomers were synthesized with ODA/ODPA as monomer and NA as end capper. The optimum reaction time in the period of polyamic acid is 40 min, the optimum imidization temperature is 80°C; DSC and TGA results show that Tg value of the oligomer increases with its NA content increasing, but decreases with its molecular weight increasing; the thermal stability decreases with its NA content increasing, but increases with its molecular weigh increasing.
| Original language | English |
|---|---|
| Pages (from-to) | 46-49 |
| Number of pages | 4 |
| Journal | Gaofenzi Cailiao Kexue Yu Gongcheng/Polymeric Materials Science and Engineering |
| Volume | 23 |
| Issue number | 6 |
| Publication status | Published - Nov 2007 |
Keywords
- Oligomer
- Polyimide
- Synthesis
- Thermal stability