Synthesis and dispersibility of derivative of 1, 3-propanediamine with nanodiamond

Gang Ke; Shi Huan; Feng Lei Huang

Synthesis and dispersibility of derivative of 1, 3-propanediamine with nanodiamond

Gang Ke, Shi Huan^*, Feng Lei Huang

^*Corresponding author for this work

School of Mechatronical Engineering

Guangzhou University

Research output: Contribution to journal › Article › peer-review

6 Citations (Scopus)

Abstract

Bad dispersibility is a major cause that hinders the application of nanodiamond (ND) severely. In this paper nanodiamond was covalently functionalized with 1, 3-propanediamine to obtain a novel derivative (ND-NH₂). FTIR results showed that the 1, 3-propanediamine molecules were covalently attached to the nanodiamonds through amide linkages. Content of the nanodiamond in the ND-NH₂ is about 29.97wt%. The ND-NH₂ dissolves not only in inorganic or organic acidic aqueous solution, but also organic solvents such as acetone, CH₂Cl₂, NMP, DMF, DMAc and DMSO. Laser Granularity and TEM results further indicated the dispersibility of the nanodiamond was much improved: the average granularity of the nanodiamond decreased from 3.301-0.166 μm by the modification of 1, 3-propanediamine. This might be a beneficial base for next study and application of nanodiamond in fields of complex electroplating and lubrication.

Original language	English
Pages (from-to)	863-866
Number of pages	4
Journal	Gongneng Cailiao/Journal of Functional Materials
Volume	40
Issue number	5
Publication status	Published - May 2009

Keywords

1, 3-propanediamine
Derivative
Dispersibility
Nanodiamond
Synthesis

Cite this

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title = "Synthesis and dispersibility of derivative of 1, 3-propanediamine with nanodiamond",

abstract = "Bad dispersibility is a major cause that hinders the application of nanodiamond (ND) severely. In this paper nanodiamond was covalently functionalized with 1, 3-propanediamine to obtain a novel derivative (ND-NH2). FTIR results showed that the 1, 3-propanediamine molecules were covalently attached to the nanodiamonds through amide linkages. Content of the nanodiamond in the ND-NH2 is about 29.97wt%. The ND-NH2 dissolves not only in inorganic or organic acidic aqueous solution, but also organic solvents such as acetone, CH2Cl2, NMP, DMF, DMAc and DMSO. Laser Granularity and TEM results further indicated the dispersibility of the nanodiamond was much improved: the average granularity of the nanodiamond decreased from 3.301-0.166 μm by the modification of 1, 3-propanediamine. This might be a beneficial base for next study and application of nanodiamond in fields of complex electroplating and lubrication.",

keywords = "1, 3-propanediamine, Derivative, Dispersibility, Nanodiamond, Synthesis",

author = "Gang Ke and Shi Huan and Huang, {Feng Lei}",

year = "2009",

month = may,

language = "English",

volume = "40",

pages = "863--866",

journal = "Gongneng Cailiao/Journal of Functional Materials",

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publisher = "Journal of Functional Materials",

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TY - JOUR

T1 - Synthesis and dispersibility of derivative of 1, 3-propanediamine with nanodiamond

AU - Ke, Gang

AU - Huan, Shi

AU - Huang, Feng Lei

PY - 2009/5

Y1 - 2009/5

N2 - Bad dispersibility is a major cause that hinders the application of nanodiamond (ND) severely. In this paper nanodiamond was covalently functionalized with 1, 3-propanediamine to obtain a novel derivative (ND-NH2). FTIR results showed that the 1, 3-propanediamine molecules were covalently attached to the nanodiamonds through amide linkages. Content of the nanodiamond in the ND-NH2 is about 29.97wt%. The ND-NH2 dissolves not only in inorganic or organic acidic aqueous solution, but also organic solvents such as acetone, CH2Cl2, NMP, DMF, DMAc and DMSO. Laser Granularity and TEM results further indicated the dispersibility of the nanodiamond was much improved: the average granularity of the nanodiamond decreased from 3.301-0.166 μm by the modification of 1, 3-propanediamine. This might be a beneficial base for next study and application of nanodiamond in fields of complex electroplating and lubrication.

AB - Bad dispersibility is a major cause that hinders the application of nanodiamond (ND) severely. In this paper nanodiamond was covalently functionalized with 1, 3-propanediamine to obtain a novel derivative (ND-NH2). FTIR results showed that the 1, 3-propanediamine molecules were covalently attached to the nanodiamonds through amide linkages. Content of the nanodiamond in the ND-NH2 is about 29.97wt%. The ND-NH2 dissolves not only in inorganic or organic acidic aqueous solution, but also organic solvents such as acetone, CH2Cl2, NMP, DMF, DMAc and DMSO. Laser Granularity and TEM results further indicated the dispersibility of the nanodiamond was much improved: the average granularity of the nanodiamond decreased from 3.301-0.166 μm by the modification of 1, 3-propanediamine. This might be a beneficial base for next study and application of nanodiamond in fields of complex electroplating and lubrication.

KW - 1, 3-propanediamine

KW - Derivative

KW - Dispersibility

KW - Nanodiamond

KW - Synthesis

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M3 - Article

AN - SCOPUS:67649208573

SN - 1001-9731

VL - 40

SP - 863

EP - 866

JO - Gongneng Cailiao/Journal of Functional Materials

JF - Gongneng Cailiao/Journal of Functional Materials

IS - 5

ER -

Synthesis and dispersibility of derivative of 1, 3-propanediamine with nanodiamond

Abstract

Keywords

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