Preparation of terephthalate-intercalated layered double hydroxides using mixed hydroxides

Wenjia Cui; Qingze Jiao; Yun Zhao; Xuefei Li; Mingji Zhou; Hongyin Shen

doi:10.1080/15533174.2011.613888

Preparation of terephthalate-intercalated layered double hydroxides using mixed hydroxides

Wenjia Cui
, Qingze Jiao^*
, Yun Zhao
, Xuefei Li
, Mingji Zhou
, Hongyin Shen

^*Corresponding author for this work

Beijing Institute of Technology

Research output: Contribution to journal › Article › peer-review

3 Citations (Scopus)

Abstract

A new method of synthesizing terephthalate-intercalated layered double hydroxides (LDHs) is reported. The key feature of this method is a reaction of freshly generated hydroxides and terephthalic acid under a hydrothermal condition. Compared with other methods, the terephthalate-intercalated LDHs synthesized using this method exhibit higher purity and higher crystallinity. XRD patterns and FT-IR spectra confirm the structure of intercalated LDHs. The effects of reaction temperature and time on the structure and morphology of the intercalated LDHs are discussed. TEM micrographs show the well-defined and uniform sized platelets of the samples.

Original language	English
Pages (from-to)	579-582
Number of pages	4
Journal	Synthesis and Reactivity in Inorganic, Metal-Organic and Nano-Metal Chemistry
Volume	42
Issue number	4
DOIs	https://doi.org/10.1080/15533174.2011.613888
Publication status	Published - 1 Apr 2012
Externally published	Yes

Keywords

intercalation
layered double hydroxides
terephthalate

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10.1080/15533174.2011.613888

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title = "Preparation of terephthalate-intercalated layered double hydroxides using mixed hydroxides",

abstract = "A new method of synthesizing terephthalate-intercalated layered double hydroxides (LDHs) is reported. The key feature of this method is a reaction of freshly generated hydroxides and terephthalic acid under a hydrothermal condition. Compared with other methods, the terephthalate-intercalated LDHs synthesized using this method exhibit higher purity and higher crystallinity. XRD patterns and FT-IR spectra confirm the structure of intercalated LDHs. The effects of reaction temperature and time on the structure and morphology of the intercalated LDHs are discussed. TEM micrographs show the well-defined and uniform sized platelets of the samples.",

keywords = "intercalation, layered double hydroxides, terephthalate",

author = "Wenjia Cui and Qingze Jiao and Yun Zhao and Xuefei Li and Mingji Zhou and Hongyin Shen",

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doi = "10.1080/15533174.2011.613888",

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T1 - Preparation of terephthalate-intercalated layered double hydroxides using mixed hydroxides

AU - Cui, Wenjia

AU - Jiao, Qingze

AU - Zhao, Yun

AU - Li, Xuefei

AU - Zhou, Mingji

AU - Shen, Hongyin

PY - 2012/4/1

Y1 - 2012/4/1

N2 - A new method of synthesizing terephthalate-intercalated layered double hydroxides (LDHs) is reported. The key feature of this method is a reaction of freshly generated hydroxides and terephthalic acid under a hydrothermal condition. Compared with other methods, the terephthalate-intercalated LDHs synthesized using this method exhibit higher purity and higher crystallinity. XRD patterns and FT-IR spectra confirm the structure of intercalated LDHs. The effects of reaction temperature and time on the structure and morphology of the intercalated LDHs are discussed. TEM micrographs show the well-defined and uniform sized platelets of the samples.

AB - A new method of synthesizing terephthalate-intercalated layered double hydroxides (LDHs) is reported. The key feature of this method is a reaction of freshly generated hydroxides and terephthalic acid under a hydrothermal condition. Compared with other methods, the terephthalate-intercalated LDHs synthesized using this method exhibit higher purity and higher crystallinity. XRD patterns and FT-IR spectra confirm the structure of intercalated LDHs. The effects of reaction temperature and time on the structure and morphology of the intercalated LDHs are discussed. TEM micrographs show the well-defined and uniform sized platelets of the samples.

KW - intercalation

KW - layered double hydroxides

KW - terephthalate

UR - https://www.scopus.com/pages/publications/84861125892

U2 - 10.1080/15533174.2011.613888

DO - 10.1080/15533174.2011.613888

M3 - Article

AN - SCOPUS:84861125892

SN - 1553-3174

VL - 42

SP - 579

EP - 582

JO - Synthesis and Reactivity in Inorganic, Metal-Organic and Nano-Metal Chemistry

JF - Synthesis and Reactivity in Inorganic, Metal-Organic and Nano-Metal Chemistry

IS - 4

ER -

Preparation of terephthalate-intercalated layered double hydroxides using mixed hydroxides

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Keywords

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