Preparation and structure characterization of 4-amino-1,2,4-triazol-5-one hydrate

Zhang Jianguo; Zhang Tonglai; Yu Kaibei

Preparation and structure characterization of 4-amino-1,2,4-triazol-5-one hydrate

Zhang Jianguo^*
, Zhang Tonglai
, Yu Kaibei

^*Corresponding author for this work

School of Mechatronical Engineering

Beijing Institute of Technology
Chengdu Br. of China Science Academy

Research output: Contribution to journal › Article › peer-review

Abstract

4-Amino-1,2,4-triazol-5-one hydrate (ATO·H₂O) was prepared and its structure was analyzed by four-circle diffraction measurement. The obtained results show that the crystal belongs to triclinic crystal system, space group P 1̄ with crystal parameters of a = 6.432(1) Å, b =6.551(1) Å, c = 6.740(1) Å, α = 68.04(1)°, β = 82.18(1)°, γ = 81.90(1)°, V = 259.7(7) Å³, Z = 2, Dc = 1.510 g/cm³, μ = 0.131 mm^-1, F(000) = 124. ATO·H₂O was characterized by FT-IR analysis, X-ray diffraction analysis and single crystal diffraction analysis.

Original language	English
Pages (from-to)	542-547
Number of pages	6
Journal	Khimiya Geterotsiklicheskikh Soedinenii
Issue number	4
Publication status	Published - 2003

Keywords

4-amino-1,2,4-triazol-5-one
Crystal structure
Molecular structure
Structure characterization

Cite this

@article{b44ea6ac442143539bdd27783a162c3b,

title = "Preparation and structure characterization of 4-amino-1,2,4-triazol-5-one hydrate",

abstract = "4-Amino-1,2,4-triazol-5-one hydrate (ATO·H2O) was prepared and its structure was analyzed by four-circle diffraction measurement. The obtained results show that the crystal belongs to triclinic crystal system, space group P {\=1} with crystal parameters of a = 6.432(1) {\AA}, b =6.551(1) {\AA}, c = 6.740(1) {\AA}, α = 68.04(1)°, β = 82.18(1)°, γ = 81.90(1)°, V = 259.7(7) {\AA}3, Z = 2, Dc = 1.510 g/cm3, μ = 0.131 mm-1, F(000) = 124. ATO·H2O was characterized by FT-IR analysis, X-ray diffraction analysis and single crystal diffraction analysis.",

keywords = "4-amino-1,2,4-triazol-5-one, Crystal structure, Molecular structure, Structure characterization",

author = "Zhang Jianguo and Zhang Tonglai and Yu Kaibei",

year = "2003",

language = "English",

pages = "542--547",

journal = "Khimiya Geterotsiklicheskikh Soedinenii",

issn = "0132-6244",

publisher = "Latvian Institute of Organic Synthesis",

number = "4",

}

TY - JOUR

T1 - Preparation and structure characterization of 4-amino-1,2,4-triazol-5-one hydrate

AU - Jianguo, Zhang

AU - Tonglai, Zhang

AU - Kaibei, Yu

PY - 2003

Y1 - 2003

N2 - 4-Amino-1,2,4-triazol-5-one hydrate (ATO·H2O) was prepared and its structure was analyzed by four-circle diffraction measurement. The obtained results show that the crystal belongs to triclinic crystal system, space group P 1̄ with crystal parameters of a = 6.432(1) Å, b =6.551(1) Å, c = 6.740(1) Å, α = 68.04(1)°, β = 82.18(1)°, γ = 81.90(1)°, V = 259.7(7) Å3, Z = 2, Dc = 1.510 g/cm3, μ = 0.131 mm-1, F(000) = 124. ATO·H2O was characterized by FT-IR analysis, X-ray diffraction analysis and single crystal diffraction analysis.

AB - 4-Amino-1,2,4-triazol-5-one hydrate (ATO·H2O) was prepared and its structure was analyzed by four-circle diffraction measurement. The obtained results show that the crystal belongs to triclinic crystal system, space group P 1̄ with crystal parameters of a = 6.432(1) Å, b =6.551(1) Å, c = 6.740(1) Å, α = 68.04(1)°, β = 82.18(1)°, γ = 81.90(1)°, V = 259.7(7) Å3, Z = 2, Dc = 1.510 g/cm3, μ = 0.131 mm-1, F(000) = 124. ATO·H2O was characterized by FT-IR analysis, X-ray diffraction analysis and single crystal diffraction analysis.

KW - 4-amino-1,2,4-triazol-5-one

KW - Crystal structure

KW - Molecular structure

KW - Structure characterization

UR - https://www.scopus.com/pages/publications/0344395622

M3 - Article

AN - SCOPUS:0344395622

SN - 0132-6244

SP - 542

EP - 547

JO - Khimiya Geterotsiklicheskikh Soedinenii

JF - Khimiya Geterotsiklicheskikh Soedinenii

IS - 4

ER -

Preparation and structure characterization of 4-amino-1,2,4-triazol-5-one hydrate

Abstract

Keywords

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