Preparation and structure characterization of 4-amino-1,2,4-triazol-5-one hydrate

Zhang Jianguo; Zhang Tonglai; Yu Kaibei

doi:10.1023/A:1024709212512

Preparation and structure characterization of 4-amino-1,2,4-triazol-5-one hydrate

Zhang Jianguo^*, Zhang Tonglai, Yu Kaibei

^*Corresponding author for this work

School of Mechatronical Engineering

Beijing Institute of Technology

Research output: Contribution to journal › Article › peer-review

5 Citations (Scopus)

Abstract

4-Amino-1,2,4-triazol-5-one hydrate (ATO·H₂O) was prepared and its structure was analyzed by four-circle diffraction measurement. The obtained results show that the crystal belongs to the triclinic crystal system, space group P 1 with crystal parameters a = 6.432(1), b = 6.551(1), c = 6.740(1) Å; α = 68.04(1), β = 82.18(1), γ = 81.90(1)°; V = 259.7(7) Å³; Z = 2; Dc = 1.510g/cm ³; μ = 0.131 mm^-1; F(000) = 124. ATO·H ₂O was characterized by FT-IR analysis, X-ray diffraction analysis, and single crystal diffraction analysis.

Original language	English
Pages (from-to)	461-466
Number of pages	6
Journal	Chemistry of Heterocyclic Compounds
Volume	39
Issue number	4
DOIs	https://doi.org/10.1023/A:1024709212512
Publication status	Published - Apr 2003

Keywords

4-amino-1,2,4-triazol-5-one
Crystal structure
Molecular structure
Structure characterization

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10.1023/A:1024709212512

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title = "Preparation and structure characterization of 4-amino-1,2,4-triazol-5-one hydrate",

abstract = "4-Amino-1,2,4-triazol-5-one hydrate (ATO·H2O) was prepared and its structure was analyzed by four-circle diffraction measurement. The obtained results show that the crystal belongs to the triclinic crystal system, space group P 1 with crystal parameters a = 6.432(1), b = 6.551(1), c = 6.740(1) {\AA}; α = 68.04(1), β = 82.18(1), γ = 81.90(1)°; V = 259.7(7) {\AA}3; Z = 2; Dc = 1.510g/cm 3; μ = 0.131 mm-1; F(000) = 124. ATO·H 2O was characterized by FT-IR analysis, X-ray diffraction analysis, and single crystal diffraction analysis.",

keywords = "4-amino-1,2,4-triazol-5-one, Crystal structure, Molecular structure, Structure characterization",

author = "Zhang Jianguo and Zhang Tonglai and Yu Kaibei",

year = "2003",

month = apr,

doi = "10.1023/A:1024709212512",

language = "English",

volume = "39",

pages = "461--466",

journal = "Chemistry of Heterocyclic Compounds",

issn = "0009-3122",

publisher = "Springer",

number = "4",

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TY - JOUR

T1 - Preparation and structure characterization of 4-amino-1,2,4-triazol-5-one hydrate

AU - Jianguo, Zhang

AU - Tonglai, Zhang

AU - Kaibei, Yu

PY - 2003/4

Y1 - 2003/4

N2 - 4-Amino-1,2,4-triazol-5-one hydrate (ATO·H2O) was prepared and its structure was analyzed by four-circle diffraction measurement. The obtained results show that the crystal belongs to the triclinic crystal system, space group P 1 with crystal parameters a = 6.432(1), b = 6.551(1), c = 6.740(1) Å; α = 68.04(1), β = 82.18(1), γ = 81.90(1)°; V = 259.7(7) Å3; Z = 2; Dc = 1.510g/cm 3; μ = 0.131 mm-1; F(000) = 124. ATO·H 2O was characterized by FT-IR analysis, X-ray diffraction analysis, and single crystal diffraction analysis.

AB - 4-Amino-1,2,4-triazol-5-one hydrate (ATO·H2O) was prepared and its structure was analyzed by four-circle diffraction measurement. The obtained results show that the crystal belongs to the triclinic crystal system, space group P 1 with crystal parameters a = 6.432(1), b = 6.551(1), c = 6.740(1) Å; α = 68.04(1), β = 82.18(1), γ = 81.90(1)°; V = 259.7(7) Å3; Z = 2; Dc = 1.510g/cm 3; μ = 0.131 mm-1; F(000) = 124. ATO·H 2O was characterized by FT-IR analysis, X-ray diffraction analysis, and single crystal diffraction analysis.

KW - 4-amino-1,2,4-triazol-5-one

KW - Crystal structure

KW - Molecular structure

KW - Structure characterization

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U2 - 10.1023/A:1024709212512

DO - 10.1023/A:1024709212512

M3 - Article

AN - SCOPUS:0142091651

SN - 0009-3122

VL - 39

SP - 461

EP - 466

JO - Chemistry of Heterocyclic Compounds

JF - Chemistry of Heterocyclic Compounds

IS - 4

ER -

Preparation and structure characterization of 4-amino-1,2,4-triazol-5-one hydrate

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Keywords

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