Preparation and molecular structure of semicarbazide picric

Li Yang; Tong Lai Zhang; Jian Guo Zhang; Bing Shao; Chang Gen Feng; Kai Bei Yu

Preparation and molecular structure of semicarbazide picric

Li Yang^*
, Tong Lai Zhang
, Jian Guo Zhang
, Bing Shao
, Chang Gen Feng
, Kai Bei Yu

^*Corresponding author for this work

School of Mechatronical Engineering

Research output: Contribution to journal › Article › peer-review

6 Citations (Scopus)

Abstract

Abstract; The preparation method and structure analysis results were obtained for the salt made from semicarbazide and picric acid. The molecular structure was characterized by elemental analysis, IR and DSC. Its crystal structure was determined by the single-crystal X-ray diffraction method with a four-circle diffractometer. The results show that the crystal is of triclinic system. Space group is Pi with crystal parameters of a =5. 024(1) Å, 6 = 10.209( I ) Å.'c = 11.551 ( 1 ) Å;a =79.00(1 )°, β = 81. 11 ( 1)°, γ=82.47(1)0;K = 571.42(14)Å³, Z =2, D_C = 1.768 g ·cm^-3, μ =0. 162 mm"', F(000) =312, R₁ = 0.032 4, Rw₂ =0.087 40.

Original language	English
Pages (from-to)	75-76
Number of pages	2
Journal	Hanneng Cailiao/Chinese Journal of Energetic Materials
Volume	9
Issue number	2
Publication status	Published - 2001

Keywords

Crystal structure
Molecular structure
Preparation
Semicarbazide picric

Cite this

@article{cbe18ce523b640e09675eedd5da9b17f,

title = "Preparation and molecular structure of semicarbazide picric",

abstract = "Abstract; The preparation method and structure analysis results were obtained for the salt made from semicarbazide and picric acid. The molecular structure was characterized by elemental analysis, IR and DSC. Its crystal structure was determined by the single-crystal X-ray diffraction method with a four-circle diffractometer. The results show that the crystal is of triclinic system. Space group is Pi with crystal parameters of a =5. 024(1) {\AA}, 6 = 10.209( I ) {\AA}.'c = 11.551 ( 1 ) {\AA};a =79.00(1 )°, β = 81. 11 ( 1)°, γ=82.47(1)0;K = 571.42(14){\AA}3, Z =2, DC = 1.768 g ·cm-3, μ =0. 162 mm{"}', F(000) =312, R1 = 0.032 4, Rw2 =0.087 40.",

keywords = "Crystal structure, Molecular structure, Preparation, Semicarbazide picric",

author = "Li Yang and Zhang, \{Tong Lai\} and Zhang, \{Jian Guo\} and Bing Shao and Feng, \{Chang Gen\} and Yu, \{Kai Bei\}",

year = "2001",

language = "English",

volume = "9",

pages = "75--76",

journal = "Hanneng Cailiao/Chinese Journal of Energetic Materials",

issn = "1006-9941",

publisher = "Institute of Chemical Materials, China Academy of Engineering Physics",

number = "2",

}

TY - JOUR

T1 - Preparation and molecular structure of semicarbazide picric

AU - Yang, Li

AU - Zhang, Tong Lai

AU - Zhang, Jian Guo

AU - Shao, Bing

AU - Feng, Chang Gen

AU - Yu, Kai Bei

PY - 2001

Y1 - 2001

N2 - Abstract; The preparation method and structure analysis results were obtained for the salt made from semicarbazide and picric acid. The molecular structure was characterized by elemental analysis, IR and DSC. Its crystal structure was determined by the single-crystal X-ray diffraction method with a four-circle diffractometer. The results show that the crystal is of triclinic system. Space group is Pi with crystal parameters of a =5. 024(1) Å, 6 = 10.209( I ) Å.'c = 11.551 ( 1 ) Å;a =79.00(1 )°, β = 81. 11 ( 1)°, γ=82.47(1)0;K = 571.42(14)Å3, Z =2, DC = 1.768 g ·cm-3, μ =0. 162 mm"', F(000) =312, R1 = 0.032 4, Rw2 =0.087 40.

AB - Abstract; The preparation method and structure analysis results were obtained for the salt made from semicarbazide and picric acid. The molecular structure was characterized by elemental analysis, IR and DSC. Its crystal structure was determined by the single-crystal X-ray diffraction method with a four-circle diffractometer. The results show that the crystal is of triclinic system. Space group is Pi with crystal parameters of a =5. 024(1) Å, 6 = 10.209( I ) Å.'c = 11.551 ( 1 ) Å;a =79.00(1 )°, β = 81. 11 ( 1)°, γ=82.47(1)0;K = 571.42(14)Å3, Z =2, DC = 1.768 g ·cm-3, μ =0. 162 mm"', F(000) =312, R1 = 0.032 4, Rw2 =0.087 40.

KW - Crystal structure

KW - Molecular structure

KW - Preparation

KW - Semicarbazide picric

UR - https://www.scopus.com/pages/publications/0034932405

M3 - Article

AN - SCOPUS:0034932405

SN - 1006-9941

VL - 9

SP - 75

EP - 76

JO - Hanneng Cailiao/Chinese Journal of Energetic Materials

JF - Hanneng Cailiao/Chinese Journal of Energetic Materials

IS - 2

ER -

Preparation and molecular structure of semicarbazide picric

Abstract

Keywords

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