Preparation and crystal structure of [Ag(TO)2]ClO4·H2O

Jian Guo Zhang; Tong Lai Zhang; Zheng Lu; Kai Bei Yu

Preparation and crystal structure of [Ag(TO)₂]ClO₄·H₂O

Jian Guo Zhang, Tong Lai Zhang^*, Zheng Lu, Kai Bei Yu

^*Corresponding author for this work

School of Mechatronical Engineering

Research output: Contribution to journal › Article › peer-review

6 Citations (Scopus)

Abstract

[Ag(TO)₂]ClO₄·H₂O was prepared by mixing the aqueous solution of 1,2,4-triazol-5-one(TO) and silver perchlorate. It was characterized by X-ray diffraction, TG-DTG, and IR measurement. The crystal is triclinic, space group P1 with a = 0.533(1) nm, b = 0.938(1) nm, c = 1.220(1) nm; α = 88.02(1)°, β = 79.50(1)°, γ = 82.86(1)°; V = 0.5953(8) nm³, Z = 2, R is 0.0281. The silver atom has a slightly bent linear coordination geometry with two nitrogen atoms.

Original language	English
Pages (from-to)	1238
Number of pages	1
Journal	Acta Chimica Sinica
Volume	57
Issue number	11
Publication status	Published - Nov 1999

Keywords

1,2,4-triazol-5-one(TO)
Crystal structure
Preparation
Silver complex

Cite this

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title = "Preparation and crystal structure of [Ag(TO)2]ClO4·H2O",

abstract = "[Ag(TO)2]ClO4·H2O was prepared by mixing the aqueous solution of 1,2,4-triazol-5-one(TO) and silver perchlorate. It was characterized by X-ray diffraction, TG-DTG, and IR measurement. The crystal is triclinic, space group P1 with a = 0.533(1) nm, b = 0.938(1) nm, c = 1.220(1) nm; α = 88.02(1)°, β = 79.50(1)°, γ = 82.86(1)°; V = 0.5953(8) nm3, Z = 2, R is 0.0281. The silver atom has a slightly bent linear coordination geometry with two nitrogen atoms.",

keywords = "1,2,4-triazol-5-one(TO), Crystal structure, Preparation, Silver complex",

author = "Zhang, \{Jian Guo\} and Zhang, \{Tong Lai\} and Zheng Lu and Yu, \{Kai Bei\}",

year = "1999",

month = nov,

language = "English",

volume = "57",

pages = "1238",

journal = "Acta Chimica Sinica",

issn = "0567-7351",

publisher = "Science Press",

number = "11",

}

TY - JOUR

T1 - Preparation and crystal structure of [Ag(TO)2]ClO4·H2O

AU - Zhang, Jian Guo

AU - Zhang, Tong Lai

AU - Lu, Zheng

AU - Yu, Kai Bei

PY - 1999/11

Y1 - 1999/11

N2 - [Ag(TO)2]ClO4·H2O was prepared by mixing the aqueous solution of 1,2,4-triazol-5-one(TO) and silver perchlorate. It was characterized by X-ray diffraction, TG-DTG, and IR measurement. The crystal is triclinic, space group P1 with a = 0.533(1) nm, b = 0.938(1) nm, c = 1.220(1) nm; α = 88.02(1)°, β = 79.50(1)°, γ = 82.86(1)°; V = 0.5953(8) nm3, Z = 2, R is 0.0281. The silver atom has a slightly bent linear coordination geometry with two nitrogen atoms.

AB - [Ag(TO)2]ClO4·H2O was prepared by mixing the aqueous solution of 1,2,4-triazol-5-one(TO) and silver perchlorate. It was characterized by X-ray diffraction, TG-DTG, and IR measurement. The crystal is triclinic, space group P1 with a = 0.533(1) nm, b = 0.938(1) nm, c = 1.220(1) nm; α = 88.02(1)°, β = 79.50(1)°, γ = 82.86(1)°; V = 0.5953(8) nm3, Z = 2, R is 0.0281. The silver atom has a slightly bent linear coordination geometry with two nitrogen atoms.

KW - 1,2,4-triazol-5-one(TO)

KW - Crystal structure

KW - Preparation

KW - Silver complex

UR - https://www.scopus.com/pages/publications/0042760480

M3 - Article

AN - SCOPUS:0042760480

SN - 0567-7351

VL - 57

SP - 1238

JO - Acta Chimica Sinica

JF - Acta Chimica Sinica

IS - 11

ER -

Preparation and crystal structure of [Ag(TO)₂]ClO₄·H₂O

Abstract

Keywords

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