Preparation and characterization of SrSnO3 nanorods

Chao Li; Youqi Zhu; Shaoming Fang; Huanxin Wang; Yanghai Gui; Lei Bi; Rongfeng Chen

doi:10.1016/j.jpcs.2011.04.001

Preparation and characterization of SrSnO₃ nanorods

Chao Li^*, Youqi Zhu, Shaoming Fang, Huanxin Wang, Yanghai Gui, Lei Bi, Rongfeng Chen

^*Corresponding author for this work

Research output: Contribution to journal › Article › peer-review

41 Citations (Scopus)

Abstract

Perovskite strontium stannate (SrSnO₃) nanorods were prepared by annealing the precursor SnSr(OH)₆ nanorods at 600 °C for 3 h. The precursor nanorods were hydrothermally synthesized at 160 °C for 16 h using Sr(NO₃)₂ and SnCl₄·5H₂O as starting materials in the presence of surfactant cetyltrimethyl ammonium bromide (CTAB). As-prepared samples were characterized by X-ray diffraction (XRD), thermogravimetric-differential thermal analysis (TG-DTA), scanning electron microscopy (SEM), transmission electron microscopy (TEM) and infrared ray spectroscopy (IR). The results show that the as-synthesized powders are made of SrSnO₃ one-dimensional nanorods of about 0.21 μm length and 100150 nm diameter. Possible formation mechanism of SrSnO₃ with nanorod structure under certain conditions was preliminarily analyzed, in which it was thought that CTAB played an important role in the formation process of the nanorod structure. Electrochemical performance of the samples versus Li metal was also evaluated for possible use in lithium-ion batteries.

Original language	English
Pages (from-to)	869-874
Number of pages	6
Journal	Journal of Physics and Chemistry of Solids
Volume	72
Issue number	7
DOIs	https://doi.org/10.1016/j.jpcs.2011.04.001
Publication status	Published - Jul 2011
Externally published	Yes

Keywords

A. Nanostructures
A. Oxides
B. Chemical synthesis
D. Electrochemical properties

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10.1016/j.jpcs.2011.04.001

Cite this

@article{06360fe41cd44f40b557207d33fe702c,

title = "Preparation and characterization of SrSnO3 nanorods",

abstract = "Perovskite strontium stannate (SrSnO3) nanorods were prepared by annealing the precursor SnSr(OH)6 nanorods at 600 °C for 3 h. The precursor nanorods were hydrothermally synthesized at 160 °C for 16 h using Sr(NO3)2 and SnCl4·5H2O as starting materials in the presence of surfactant cetyltrimethyl ammonium bromide (CTAB). As-prepared samples were characterized by X-ray diffraction (XRD), thermogravimetric-differential thermal analysis (TG-DTA), scanning electron microscopy (SEM), transmission electron microscopy (TEM) and infrared ray spectroscopy (IR). The results show that the as-synthesized powders are made of SrSnO3 one-dimensional nanorods of about 0.21 μm length and 100150 nm diameter. Possible formation mechanism of SrSnO3 with nanorod structure under certain conditions was preliminarily analyzed, in which it was thought that CTAB played an important role in the formation process of the nanorod structure. Electrochemical performance of the samples versus Li metal was also evaluated for possible use in lithium-ion batteries.",

keywords = "A. Nanostructures, A. Oxides, B. Chemical synthesis, D. Electrochemical properties",

author = "Chao Li and Youqi Zhu and Shaoming Fang and Huanxin Wang and Yanghai Gui and Lei Bi and Rongfeng Chen",

year = "2011",

month = jul,

doi = "10.1016/j.jpcs.2011.04.001",

language = "English",

volume = "72",

pages = "869--874",

journal = "Journal of Physics and Chemistry of Solids",

issn = "0022-3697",

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}

TY - JOUR

T1 - Preparation and characterization of SrSnO3 nanorods

AU - Li, Chao

AU - Zhu, Youqi

AU - Fang, Shaoming

AU - Wang, Huanxin

AU - Gui, Yanghai

AU - Bi, Lei

AU - Chen, Rongfeng

PY - 2011/7

Y1 - 2011/7

N2 - Perovskite strontium stannate (SrSnO3) nanorods were prepared by annealing the precursor SnSr(OH)6 nanorods at 600 °C for 3 h. The precursor nanorods were hydrothermally synthesized at 160 °C for 16 h using Sr(NO3)2 and SnCl4·5H2O as starting materials in the presence of surfactant cetyltrimethyl ammonium bromide (CTAB). As-prepared samples were characterized by X-ray diffraction (XRD), thermogravimetric-differential thermal analysis (TG-DTA), scanning electron microscopy (SEM), transmission electron microscopy (TEM) and infrared ray spectroscopy (IR). The results show that the as-synthesized powders are made of SrSnO3 one-dimensional nanorods of about 0.21 μm length and 100150 nm diameter. Possible formation mechanism of SrSnO3 with nanorod structure under certain conditions was preliminarily analyzed, in which it was thought that CTAB played an important role in the formation process of the nanorod structure. Electrochemical performance of the samples versus Li metal was also evaluated for possible use in lithium-ion batteries.

AB - Perovskite strontium stannate (SrSnO3) nanorods were prepared by annealing the precursor SnSr(OH)6 nanorods at 600 °C for 3 h. The precursor nanorods were hydrothermally synthesized at 160 °C for 16 h using Sr(NO3)2 and SnCl4·5H2O as starting materials in the presence of surfactant cetyltrimethyl ammonium bromide (CTAB). As-prepared samples were characterized by X-ray diffraction (XRD), thermogravimetric-differential thermal analysis (TG-DTA), scanning electron microscopy (SEM), transmission electron microscopy (TEM) and infrared ray spectroscopy (IR). The results show that the as-synthesized powders are made of SrSnO3 one-dimensional nanorods of about 0.21 μm length and 100150 nm diameter. Possible formation mechanism of SrSnO3 with nanorod structure under certain conditions was preliminarily analyzed, in which it was thought that CTAB played an important role in the formation process of the nanorod structure. Electrochemical performance of the samples versus Li metal was also evaluated for possible use in lithium-ion batteries.

KW - A. Nanostructures

KW - A. Oxides

KW - B. Chemical synthesis

KW - D. Electrochemical properties

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