Preparation and characterization of amino-functionalized multi-walled carbon nanotubes

Bing Zhi Guo; Yun Zhao; Han Sheng Li; Qing Ze Jiao

doi:10.3969/j.issn.1001-4861.2013.00194

Preparation and characterization of amino-functionalized multi-walled carbon nanotubes

Bing Zhi Guo
, Yun Zhao
, Han Sheng Li
, Qing Ze Jiao

School of Chemistry and Chemical Engineering

Beijing Institute of Technology

Research output: Contribution to journal › Article › peer-review

4 Citations (Scopus)

Abstract

Cyano functional groups were covalently attached to the surface of multi-walled carbon nanotubes (MWNTs) by free radical addition of AIBN, then Al-NiCl₂·6H₂O-THF system was used to reduce the cyano to obtain aminofunctionalized carbon nanotubes. he structure and morphology of amino-functionalized M s were characterized by Raman spectroscopy, thermal gravimetric analysis, X-ray photoelectron spectroscopy and transmission electron microscopy. he results showed that amino group was linked to the surface of MWNTs and approximately 17.1 of every 1 000 carbon atoms on the surface of MWNTs were grafted to amino groups.

Original language	English
Pages (from-to)	1825-1829
Number of pages	5
Journal	Chinese Journal of Inorganic Chemistry
Volume	29
Issue number	9
DOIs	https://doi.org/10.3969/j.issn.1001-4861.2013.00194
Publication status	Published - Sept 2013

Keywords

Amino
Carbon nanotubes
Functionalization

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10.3969/j.issn.1001-4861.2013.00194

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title = "Preparation and characterization of amino-functionalized multi-walled carbon nanotubes",

abstract = "Cyano functional groups were covalently attached to the surface of multi-walled carbon nanotubes (MWNTs) by free radical addition of AIBN, then Al-NiCl2·6H2O-THF system was used to reduce the cyano to obtain aminofunctionalized carbon nanotubes. he structure and morphology of amino-functionalized M s were characterized by Raman spectroscopy, thermal gravimetric analysis, X-ray photoelectron spectroscopy and transmission electron microscopy. he results showed that amino group was linked to the surface of MWNTs and approximately 17.1 of every 1 000 carbon atoms on the surface of MWNTs were grafted to amino groups.",

keywords = "Amino, Carbon nanotubes, Functionalization",

author = "Guo, \{Bing Zhi\} and Yun Zhao and Li, \{Han Sheng\} and Jiao, \{Qing Ze\}",

year = "2013",

month = sep,

doi = "10.3969/j.issn.1001-4861.2013.00194",

language = "English",

volume = "29",

pages = "1825--1829",

journal = "Chinese Journal of Inorganic Chemistry",

issn = "1001-4861",

publisher = "Chinese Chemical Society",

number = "9",

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TY - JOUR

T1 - Preparation and characterization of amino-functionalized multi-walled carbon nanotubes

AU - Guo, Bing Zhi

AU - Zhao, Yun

AU - Li, Han Sheng

AU - Jiao, Qing Ze

PY - 2013/9

Y1 - 2013/9

N2 - Cyano functional groups were covalently attached to the surface of multi-walled carbon nanotubes (MWNTs) by free radical addition of AIBN, then Al-NiCl2·6H2O-THF system was used to reduce the cyano to obtain aminofunctionalized carbon nanotubes. he structure and morphology of amino-functionalized M s were characterized by Raman spectroscopy, thermal gravimetric analysis, X-ray photoelectron spectroscopy and transmission electron microscopy. he results showed that amino group was linked to the surface of MWNTs and approximately 17.1 of every 1 000 carbon atoms on the surface of MWNTs were grafted to amino groups.

AB - Cyano functional groups were covalently attached to the surface of multi-walled carbon nanotubes (MWNTs) by free radical addition of AIBN, then Al-NiCl2·6H2O-THF system was used to reduce the cyano to obtain aminofunctionalized carbon nanotubes. he structure and morphology of amino-functionalized M s were characterized by Raman spectroscopy, thermal gravimetric analysis, X-ray photoelectron spectroscopy and transmission electron microscopy. he results showed that amino group was linked to the surface of MWNTs and approximately 17.1 of every 1 000 carbon atoms on the surface of MWNTs were grafted to amino groups.

KW - Amino

KW - Carbon nanotubes

KW - Functionalization

UR - https://www.scopus.com/pages/publications/84940322635

U2 - 10.3969/j.issn.1001-4861.2013.00194

DO - 10.3969/j.issn.1001-4861.2013.00194

M3 - Article

AN - SCOPUS:84940322635

SN - 1001-4861

VL - 29

SP - 1825

EP - 1829

JO - Chinese Journal of Inorganic Chemistry

JF - Chinese Journal of Inorganic Chemistry

IS - 9

ER -

Preparation and characterization of amino-functionalized multi-walled carbon nanotubes

Abstract

Keywords

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