Fabrication, characterisation, and structure of Nd2Zr2O7 microbelts prepared by electrospinning method

Zhiliang Zhou; Debao Liu; Zelong Wang; Baosheng Xu

doi:10.1016/j.matlet.2022.133105

Fabrication, characterisation, and structure of Nd₂Zr₂O₇ microbelts prepared by electrospinning method

Zhiliang Zhou, Debao Liu, Zelong Wang, Baosheng Xu^*

^*Corresponding author for this work

Beijing Institute of Technology

Research output: Contribution to journal › Article › peer-review

1 Citation (Scopus)

Abstract

Nd₂Zr₂O₇ microbelts were successfully prepared by simple electrospinning paired with calcination. The composition, microstructure, and structure of the as-prepared Nd₂Zr₂O₇ microbelts were systematically characterized through a combination of characterisations, such as XRD, SEM, TEM, FT-IR, and TG-DSC techniques. Results indicated that the as-prepared Nd₂Zr₂O₇ microbelts had a pyrochlore-type crystal structure and uniform size with about 10 μm thickness. Moreover, a feasible formation mechanism of the Nd₂Zr₂O₇ microbelts was discussed. The present procedure can be expanded to develop other rare-earth zirconate materials with belt structure.

Original language	English
Article number	133105
Journal	Materials Letters
Volume	329
DOIs	https://doi.org/10.1016/j.matlet.2022.133105
Publication status	Published - 15 Dec 2022
Externally published	Yes

Keywords

Crystal structure
Electrospinning
Formation mechanism
Microstructure

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10.1016/j.matlet.2022.133105

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title = "Fabrication, characterisation, and structure of Nd2Zr2O7 microbelts prepared by electrospinning method",

abstract = "Nd2Zr2O7 microbelts were successfully prepared by simple electrospinning paired with calcination. The composition, microstructure, and structure of the as-prepared Nd2Zr2O7 microbelts were systematically characterized through a combination of characterisations, such as XRD, SEM, TEM, FT-IR, and TG-DSC techniques. Results indicated that the as-prepared Nd2Zr2O7 microbelts had a pyrochlore-type crystal structure and uniform size with about 10 μm thickness. Moreover, a feasible formation mechanism of the Nd2Zr2O7 microbelts was discussed. The present procedure can be expanded to develop other rare-earth zirconate materials with belt structure.",

keywords = "Crystal structure, Electrospinning, Formation mechanism, Microstructure",

author = "Zhiliang Zhou and Debao Liu and Zelong Wang and Baosheng Xu",

note = "Publisher Copyright: {\textcopyright} 2022",

year = "2022",

month = dec,

day = "15",

doi = "10.1016/j.matlet.2022.133105",

language = "English",

volume = "329",

journal = "Materials Letters",

issn = "0167-577X",

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TY - JOUR

T1 - Fabrication, characterisation, and structure of Nd2Zr2O7 microbelts prepared by electrospinning method

AU - Zhou, Zhiliang

AU - Liu, Debao

AU - Wang, Zelong

AU - Xu, Baosheng

PY - 2022/12/15

Y1 - 2022/12/15

N2 - Nd2Zr2O7 microbelts were successfully prepared by simple electrospinning paired with calcination. The composition, microstructure, and structure of the as-prepared Nd2Zr2O7 microbelts were systematically characterized through a combination of characterisations, such as XRD, SEM, TEM, FT-IR, and TG-DSC techniques. Results indicated that the as-prepared Nd2Zr2O7 microbelts had a pyrochlore-type crystal structure and uniform size with about 10 μm thickness. Moreover, a feasible formation mechanism of the Nd2Zr2O7 microbelts was discussed. The present procedure can be expanded to develop other rare-earth zirconate materials with belt structure.

AB - Nd2Zr2O7 microbelts were successfully prepared by simple electrospinning paired with calcination. The composition, microstructure, and structure of the as-prepared Nd2Zr2O7 microbelts were systematically characterized through a combination of characterisations, such as XRD, SEM, TEM, FT-IR, and TG-DSC techniques. Results indicated that the as-prepared Nd2Zr2O7 microbelts had a pyrochlore-type crystal structure and uniform size with about 10 μm thickness. Moreover, a feasible formation mechanism of the Nd2Zr2O7 microbelts was discussed. The present procedure can be expanded to develop other rare-earth zirconate materials with belt structure.

KW - Crystal structure

KW - Electrospinning

KW - Formation mechanism

KW - Microstructure

UR - https://www.scopus.com/pages/publications/85139734166

U2 - 10.1016/j.matlet.2022.133105

DO - 10.1016/j.matlet.2022.133105

M3 - Article

AN - SCOPUS:85139734166

SN - 0167-577X

VL - 329

JO - Materials Letters

JF - Materials Letters

M1 - 133105

ER -

Fabrication, characterisation, and structure of Nd₂Zr₂O₇ microbelts prepared by electrospinning method

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Keywords

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