Determination of acid number in hexanitrohexaazaisowurtane by method of titration

Ying Zhang; Shu Sen Chen; Shao Hua Jin; Yan Shan Shi

Determination of acid number in hexanitrohexaazaisowurtane by method of titration

Ying Zhang^*
, Shu Sen Chen
, Shao Hua Jin
, Yan Shan Shi

^*Corresponding author for this work

School of Material Science and Engineering

Beijing Institute of Technology
Linfen Fire Detachment of Shanxi

Research output: Contribution to journal › Article › peer-review

1 Citation (Scopus)

Abstract

Method of acid-alkali titration is traditional analysis method. It is typical of manipulation easy, little error and excellent accuracy. In this paper, by using the method of acid-alkali titration, the acid number for ε-hexanitrohexaazaisowurtane (HNIW) obtained in two system (nitric acid and ethyl acetate and chloroform) was determination respectively. Different conditions were determined. For ε-HNIW prepared in nitric acid system, titration conditions are 5-6 g HNIW with 80 mL acetone as solvent and neutral red-methylene blue as indicator. For ε-HNIW prepared in EtOAc-CHCl₃ system, conditions are 5-6 g HNIW with 50 mL acetone as solvent and resorcin blue as indicator.

Original language	English
Pages (from-to)	397-399
Number of pages	3
Journal	Hanneng Cailiao/Chinese Journal of Energetic Materials
Volume	14
Issue number	5
Publication status	Published - Oct 2006

Keywords

Acid number
Analysis chemistry
Hexanitrohexaazaisowurtane
Indicator
Titration

Cite this

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title = "Determination of acid number in hexanitrohexaazaisowurtane by method of titration",

abstract = "Method of acid-alkali titration is traditional analysis method. It is typical of manipulation easy, little error and excellent accuracy. In this paper, by using the method of acid-alkali titration, the acid number for ε-hexanitrohexaazaisowurtane (HNIW) obtained in two system (nitric acid and ethyl acetate and chloroform) was determination respectively. Different conditions were determined. For ε-HNIW prepared in nitric acid system, titration conditions are 5-6 g HNIW with 80 mL acetone as solvent and neutral red-methylene blue as indicator. For ε-HNIW prepared in EtOAc-CHCl3 system, conditions are 5-6 g HNIW with 50 mL acetone as solvent and resorcin blue as indicator.",

keywords = "Acid number, Analysis chemistry, Hexanitrohexaazaisowurtane, Indicator, Titration",

author = "Ying Zhang and Chen, \{Shu Sen\} and Jin, \{Shao Hua\} and Shi, \{Yan Shan\}",

year = "2006",

month = oct,

language = "English",

volume = "14",

pages = "397--399",

journal = "Hanneng Cailiao/Chinese Journal of Energetic Materials",

issn = "1006-9941",

publisher = "Institute of Chemical Materials, China Academy of Engineering Physics",

number = "5",

}

TY - JOUR

T1 - Determination of acid number in hexanitrohexaazaisowurtane by method of titration

AU - Zhang, Ying

AU - Chen, Shu Sen

AU - Jin, Shao Hua

AU - Shi, Yan Shan

PY - 2006/10

Y1 - 2006/10

N2 - Method of acid-alkali titration is traditional analysis method. It is typical of manipulation easy, little error and excellent accuracy. In this paper, by using the method of acid-alkali titration, the acid number for ε-hexanitrohexaazaisowurtane (HNIW) obtained in two system (nitric acid and ethyl acetate and chloroform) was determination respectively. Different conditions were determined. For ε-HNIW prepared in nitric acid system, titration conditions are 5-6 g HNIW with 80 mL acetone as solvent and neutral red-methylene blue as indicator. For ε-HNIW prepared in EtOAc-CHCl3 system, conditions are 5-6 g HNIW with 50 mL acetone as solvent and resorcin blue as indicator.

AB - Method of acid-alkali titration is traditional analysis method. It is typical of manipulation easy, little error and excellent accuracy. In this paper, by using the method of acid-alkali titration, the acid number for ε-hexanitrohexaazaisowurtane (HNIW) obtained in two system (nitric acid and ethyl acetate and chloroform) was determination respectively. Different conditions were determined. For ε-HNIW prepared in nitric acid system, titration conditions are 5-6 g HNIW with 80 mL acetone as solvent and neutral red-methylene blue as indicator. For ε-HNIW prepared in EtOAc-CHCl3 system, conditions are 5-6 g HNIW with 50 mL acetone as solvent and resorcin blue as indicator.

KW - Acid number

KW - Analysis chemistry

KW - Hexanitrohexaazaisowurtane

KW - Indicator

KW - Titration

UR - https://www.scopus.com/pages/publications/33846149309

M3 - Article

AN - SCOPUS:33846149309

SN - 1006-9941

VL - 14

SP - 397

EP - 399

JO - Hanneng Cailiao/Chinese Journal of Energetic Materials

JF - Hanneng Cailiao/Chinese Journal of Energetic Materials

IS - 5

ER -

Determination of acid number in hexanitrohexaazaisowurtane by method of titration

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Keywords

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