Crystal structure of 8β-hydroxyeremophil-7(11)-ene-12, 8α(4β,6α)-diolide

Hui Qing Xue; Hui Feng Xue; Biao Wu; Han Qing Wang; Xue Lei Xin; Shui Xian Wu

doi:10.1360/cjcp2006.19(6).519.4

Crystal structure of 8β-hydroxyeremophil-7(11)-ene-12, 8α(4β,6α)-diolide

Hui Qing Xue
, Hui Feng Xue
, Biao Wu
, Han Qing Wang^*
, Xue Lei Xin
, Shui Xian Wu

^*Corresponding author for this work

Research output: Contribution to journal › Article › peer-review

4 Citations (Scopus)

Abstract

8β-hydroxyeremophil-7(11)-ene-12,8α(4β,6α)-diolide was isolated from the Ligularia intermedia and characterized by MS, multi NMR and X-ray single crystal diffraction. Its crystal structure was determined as in a orthorhombic type, with space group P2₁2₁2₁ with a=6.8519(5), b=10.7191(8), c=18.5942(14) Å, V=1365.67(18) Å³, Z=4, and the calculated density is 1.354 mg/m³. F(000)=592, μ=0.101 mm^-1.

Original language	English
Pages (from-to)	519-522+ii
Journal	Chinese Journal of Chemical Physics
Volume	19
Issue number	6
DOIs	https://doi.org/10.1360/cjcp2006.19(6).519.4
Publication status	Published - 27 Dec 2006
Externally published	Yes

Keywords

Crystal structure
Isolation
Ligularia intermedia
X-ray diffraction

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10.1360/cjcp2006.19(6).519.4

Cite this

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title = "Crystal structure of 8β-hydroxyeremophil-7(11)-ene-12, 8α(4β,6α)-diolide",

abstract = "8β-hydroxyeremophil-7(11)-ene-12,8α(4β,6α)-diolide was isolated from the Ligularia intermedia and characterized by MS, multi NMR and X-ray single crystal diffraction. Its crystal structure was determined as in a orthorhombic type, with space group P212121 with a=6.8519(5), b=10.7191(8), c=18.5942(14) {\AA}, V=1365.67(18) {\AA}3, Z=4, and the calculated density is 1.354 mg/m3. F(000)=592, μ=0.101 mm-1.",

keywords = "Crystal structure, Isolation, Ligularia intermedia, X-ray diffraction",

author = "Xue, \{Hui Qing\} and Xue, \{Hui Feng\} and Biao Wu and Wang, \{Han Qing\} and Xin, \{Xue Lei\} and Wu, \{Shui Xian\}",

year = "2006",

month = dec,

day = "27",

doi = "10.1360/cjcp2006.19(6).519.4",

language = "English",

volume = "19",

pages = "519--522+ii",

journal = "Chinese Journal of Chemical Physics",

issn = "1674-0068",

publisher = "American Institute of Physics",

number = "6",

}

TY - JOUR

T1 - Crystal structure of 8β-hydroxyeremophil-7(11)-ene-12, 8α(4β,6α)-diolide

AU - Xue, Hui Qing

AU - Xue, Hui Feng

AU - Wu, Biao

AU - Wang, Han Qing

AU - Xin, Xue Lei

AU - Wu, Shui Xian

PY - 2006/12/27

Y1 - 2006/12/27

N2 - 8β-hydroxyeremophil-7(11)-ene-12,8α(4β,6α)-diolide was isolated from the Ligularia intermedia and characterized by MS, multi NMR and X-ray single crystal diffraction. Its crystal structure was determined as in a orthorhombic type, with space group P212121 with a=6.8519(5), b=10.7191(8), c=18.5942(14) Å, V=1365.67(18) Å3, Z=4, and the calculated density is 1.354 mg/m3. F(000)=592, μ=0.101 mm-1.

AB - 8β-hydroxyeremophil-7(11)-ene-12,8α(4β,6α)-diolide was isolated from the Ligularia intermedia and characterized by MS, multi NMR and X-ray single crystal diffraction. Its crystal structure was determined as in a orthorhombic type, with space group P212121 with a=6.8519(5), b=10.7191(8), c=18.5942(14) Å, V=1365.67(18) Å3, Z=4, and the calculated density is 1.354 mg/m3. F(000)=592, μ=0.101 mm-1.

KW - Crystal structure

KW - Isolation

KW - Ligularia intermedia

KW - X-ray diffraction

UR - https://www.scopus.com/pages/publications/33847123620

U2 - 10.1360/cjcp2006.19(6).519.4

DO - 10.1360/cjcp2006.19(6).519.4

M3 - Article

AN - SCOPUS:33847123620

SN - 1674-0068

VL - 19

SP - 519-522+ii

JO - Chinese Journal of Chemical Physics

JF - Chinese Journal of Chemical Physics

IS - 6

ER -

Crystal structure of 8β-hydroxyeremophil-7(11)-ene-12, 8α(4β,6α)-diolide

Abstract

Keywords

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