Controlled solvothermal synthesis and structural characterization of antimony telluride nanoforks

Shufeng Shi; Minhua Cao; Changwen Hu

doi:10.1021/cg800551u

Controlled solvothermal synthesis and structural characterization of antimony telluride nanoforks

Shufeng Shi
, Minhua Cao^*
, Changwen Hu

^*Corresponding author for this work

Northeast Normal University
Beijing Institute of Technology

Research output: Contribution to journal › Article › peer-review

27 Citations (Scopus)

Abstract

High-quality Sb₂Te₃ nanoforks have been first successfully prepared by a simple wet chemical method under solvothermal conditions. Here, ethylene glycol has been used not only as a solvent, but also as a reducing agent. The nitric acid used has been proven to play an important role in the formation of such a unique shape. The shape and size of Sb2Te3 nanoforks can be well controlled by adjusting the experiment parameters. X-ray diffraction (XRD), X-ray photoelectron spectra (XPS), scanning electron microscopy (SEM), transmission electron microscopy (TEM), and high-resolution transmission electron microscopy (HRTEM) were used to characterize the as-synthesized samples.

Original language	English
Pages (from-to)	2057-2060
Number of pages	4
Journal	Crystal Growth and Design
Volume	9
Issue number	5
DOIs	https://doi.org/10.1021/cg800551u
Publication status	Published - 6 May 2009
Externally published	Yes

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title = "Controlled solvothermal synthesis and structural characterization of antimony telluride nanoforks",

abstract = "High-quality Sb2Te3 nanoforks have been first successfully prepared by a simple wet chemical method under solvothermal conditions. Here, ethylene glycol has been used not only as a solvent, but also as a reducing agent. The nitric acid used has been proven to play an important role in the formation of such a unique shape. The shape and size of Sb2Te3 nanoforks can be well controlled by adjusting the experiment parameters. X-ray diffraction (XRD), X-ray photoelectron spectra (XPS), scanning electron microscopy (SEM), transmission electron microscopy (TEM), and high-resolution transmission electron microscopy (HRTEM) were used to characterize the as-synthesized samples.",

author = "Shufeng Shi and Minhua Cao and Changwen Hu",

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AU - Shi, Shufeng

AU - Cao, Minhua

AU - Hu, Changwen

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N2 - High-quality Sb2Te3 nanoforks have been first successfully prepared by a simple wet chemical method under solvothermal conditions. Here, ethylene glycol has been used not only as a solvent, but also as a reducing agent. The nitric acid used has been proven to play an important role in the formation of such a unique shape. The shape and size of Sb2Te3 nanoforks can be well controlled by adjusting the experiment parameters. X-ray diffraction (XRD), X-ray photoelectron spectra (XPS), scanning electron microscopy (SEM), transmission electron microscopy (TEM), and high-resolution transmission electron microscopy (HRTEM) were used to characterize the as-synthesized samples.

AB - High-quality Sb2Te3 nanoforks have been first successfully prepared by a simple wet chemical method under solvothermal conditions. Here, ethylene glycol has been used not only as a solvent, but also as a reducing agent. The nitric acid used has been proven to play an important role in the formation of such a unique shape. The shape and size of Sb2Te3 nanoforks can be well controlled by adjusting the experiment parameters. X-ray diffraction (XRD), X-ray photoelectron spectra (XPS), scanning electron microscopy (SEM), transmission electron microscopy (TEM), and high-resolution transmission electron microscopy (HRTEM) were used to characterize the as-synthesized samples.

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JF - Crystal Growth and Design

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Controlled solvothermal synthesis and structural characterization of antimony telluride nanoforks

Abstract

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