AIBN-Promoted Synthesis of Bibenzo[ b][1,4]thiazines by the Condensation of 2,2′-Dithiodianiline with Methyl Aryl Ketones

Xianqiang Huang; Nianxin Rong; Pengfei Li; Guodong Shen; Qiang Li; Nana Xin; Chuansheng Cui; Jichui Cui; Bingchuan Yang; Dacheng Li; Changqiu Zhao; Jianmin Dou; Bo Wang

doi:10.1021/acs.orglett.8b01238

AIBN-Promoted Synthesis of Bibenzo[ b][1,4]thiazines by the Condensation of 2,2′-Dithiodianiline with Methyl Aryl Ketones

Xianqiang Huang, Nianxin Rong, Pengfei Li^*, Guodong Shen, Qiang Li, Nana Xin, Chuansheng Cui, Jichui Cui, Bingchuan Yang, Dacheng Li, Changqiu Zhao, Jianmin Dou, Bo Wang

^*Corresponding author for this work

School of Chemistry and Chemical Engineering

Research output: Contribution to journal › Article › peer-review

27 Citations (Scopus)

Abstract

A series of bibenzo[b][1,4]thiazines with various functional groups has been synthesized by a free-radical condensation reaction. Bibenzo[b][1,4]thiazines were obtained in moderate to good yield (up to 85%) through a one-step reaction of readily available 2,2′-dithiodianiline and methyl aryl ketones with AIBN as radical initiator in HOAc. Bibenzo[b][1,4]thiazines exhibit diversiform solid-state packing.

Original language	English
Pages (from-to)	3332-3336
Number of pages	5
Journal	Organic Letters
Volume	20
Issue number	11
DOIs	https://doi.org/10.1021/acs.orglett.8b01238
Publication status	Published - 1 Jun 2018

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@article{c53601b1239d443c803c2f0f848d6c10,

title = "AIBN-Promoted Synthesis of Bibenzo[ b][1,4]thiazines by the Condensation of 2,2′-Dithiodianiline with Methyl Aryl Ketones",

abstract = "A series of bibenzo[b][1,4]thiazines with various functional groups has been synthesized by a free-radical condensation reaction. Bibenzo[b][1,4]thiazines were obtained in moderate to good yield (up to 85\%) through a one-step reaction of readily available 2,2′-dithiodianiline and methyl aryl ketones with AIBN as radical initiator in HOAc. Bibenzo[b][1,4]thiazines exhibit diversiform solid-state packing.",

author = "Xianqiang Huang and Nianxin Rong and Pengfei Li and Guodong Shen and Qiang Li and Nana Xin and Chuansheng Cui and Jichui Cui and Bingchuan Yang and Dacheng Li and Changqiu Zhao and Jianmin Dou and Bo Wang",

note = "Publisher Copyright: {\textcopyright} 2018 American Chemical Society.",

year = "2018",

month = jun,

day = "1",

doi = "10.1021/acs.orglett.8b01238",

language = "English",

volume = "20",

pages = "3332--3336",

journal = "Organic Letters",

issn = "1523-7060",

publisher = "American Chemical Society",

number = "11",

}

TY - JOUR

T1 - AIBN-Promoted Synthesis of Bibenzo[ b][1,4]thiazines by the Condensation of 2,2′-Dithiodianiline with Methyl Aryl Ketones

AU - Huang, Xianqiang

AU - Rong, Nianxin

AU - Li, Pengfei

AU - Shen, Guodong

AU - Li, Qiang

AU - Xin, Nana

AU - Cui, Chuansheng

AU - Cui, Jichui

AU - Yang, Bingchuan

AU - Li, Dacheng

AU - Zhao, Changqiu

AU - Dou, Jianmin

AU - Wang, Bo

PY - 2018/6/1

Y1 - 2018/6/1

N2 - A series of bibenzo[b][1,4]thiazines with various functional groups has been synthesized by a free-radical condensation reaction. Bibenzo[b][1,4]thiazines were obtained in moderate to good yield (up to 85%) through a one-step reaction of readily available 2,2′-dithiodianiline and methyl aryl ketones with AIBN as radical initiator in HOAc. Bibenzo[b][1,4]thiazines exhibit diversiform solid-state packing.

AB - A series of bibenzo[b][1,4]thiazines with various functional groups has been synthesized by a free-radical condensation reaction. Bibenzo[b][1,4]thiazines were obtained in moderate to good yield (up to 85%) through a one-step reaction of readily available 2,2′-dithiodianiline and methyl aryl ketones with AIBN as radical initiator in HOAc. Bibenzo[b][1,4]thiazines exhibit diversiform solid-state packing.

UR - https://www.scopus.com/pages/publications/85048039420

U2 - 10.1021/acs.orglett.8b01238

DO - 10.1021/acs.orglett.8b01238

M3 - Article

C2 - 29771129

AN - SCOPUS:85048039420

SN - 1523-7060

VL - 20

SP - 3332

EP - 3336

JO - Organic Letters

JF - Organic Letters

IS - 11

ER -

AIBN-Promoted Synthesis of Bibenzo[ b][1,4]thiazines by the Condensation of 2,2′-Dithiodianiline with Methyl Aryl Ketones

Abstract

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