Determination of acid number in hexanitrohexaazaisowurtane by method of titration

Ying Zhang; Shu Sen Chen; Shao Hua Jin; Yan Shan Shi

Determination of acid number in hexanitrohexaazaisowurtane by method of titration

Ying Zhang^*, Shu Sen Chen, Shao Hua Jin, Yan Shan Shi

^*此作品的通讯作者

材料学院

科研成果: 期刊稿件 › 文章 › 同行评审

1 引用（Scopus）

摘要

Method of acid-alkali titration is traditional analysis method. It is typical of manipulation easy, little error and excellent accuracy. In this paper, by using the method of acid-alkali titration, the acid number for ε-hexanitrohexaazaisowurtane (HNIW) obtained in two system (nitric acid and ethyl acetate and chloroform) was determination respectively. Different conditions were determined. For ε-HNIW prepared in nitric acid system, titration conditions are 5-6 g HNIW with 80 mL acetone as solvent and neutral red-methylene blue as indicator. For ε-HNIW prepared in EtOAc-CHCl₃ system, conditions are 5-6 g HNIW with 50 mL acetone as solvent and resorcin blue as indicator.

源语言	英语
页（从-至）	397-399
页数	3
期刊	Hanneng Cailiao/Chinese Journal of Energetic Materials
卷	14
期	5
出版状态	已出版 - 10月 2006

其它文件与链接

链接到 Scopus 的出版物

引用此

@article{8ce9e7a49a3f40569f20fa904a1d436d,

title = "Determination of acid number in hexanitrohexaazaisowurtane by method of titration",

abstract = "Method of acid-alkali titration is traditional analysis method. It is typical of manipulation easy, little error and excellent accuracy. In this paper, by using the method of acid-alkali titration, the acid number for ε-hexanitrohexaazaisowurtane (HNIW) obtained in two system (nitric acid and ethyl acetate and chloroform) was determination respectively. Different conditions were determined. For ε-HNIW prepared in nitric acid system, titration conditions are 5-6 g HNIW with 80 mL acetone as solvent and neutral red-methylene blue as indicator. For ε-HNIW prepared in EtOAc-CHCl3 system, conditions are 5-6 g HNIW with 50 mL acetone as solvent and resorcin blue as indicator.",

keywords = "Acid number, Analysis chemistry, Hexanitrohexaazaisowurtane, Indicator, Titration",

author = "Ying Zhang and Chen, {Shu Sen} and Jin, {Shao Hua} and Shi, {Yan Shan}",

year = "2006",

month = oct,

language = "English",

volume = "14",

pages = "397--399",

journal = "Hanneng Cailiao/Chinese Journal of Energetic Materials",

issn = "1006-9941",

publisher = "Chinese Academy of Engineering Physics",

number = "5",

}

TY - JOUR

T1 - Determination of acid number in hexanitrohexaazaisowurtane by method of titration

AU - Zhang, Ying

AU - Chen, Shu Sen

AU - Jin, Shao Hua

AU - Shi, Yan Shan

PY - 2006/10

Y1 - 2006/10

N2 - Method of acid-alkali titration is traditional analysis method. It is typical of manipulation easy, little error and excellent accuracy. In this paper, by using the method of acid-alkali titration, the acid number for ε-hexanitrohexaazaisowurtane (HNIW) obtained in two system (nitric acid and ethyl acetate and chloroform) was determination respectively. Different conditions were determined. For ε-HNIW prepared in nitric acid system, titration conditions are 5-6 g HNIW with 80 mL acetone as solvent and neutral red-methylene blue as indicator. For ε-HNIW prepared in EtOAc-CHCl3 system, conditions are 5-6 g HNIW with 50 mL acetone as solvent and resorcin blue as indicator.

AB - Method of acid-alkali titration is traditional analysis method. It is typical of manipulation easy, little error and excellent accuracy. In this paper, by using the method of acid-alkali titration, the acid number for ε-hexanitrohexaazaisowurtane (HNIW) obtained in two system (nitric acid and ethyl acetate and chloroform) was determination respectively. Different conditions were determined. For ε-HNIW prepared in nitric acid system, titration conditions are 5-6 g HNIW with 80 mL acetone as solvent and neutral red-methylene blue as indicator. For ε-HNIW prepared in EtOAc-CHCl3 system, conditions are 5-6 g HNIW with 50 mL acetone as solvent and resorcin blue as indicator.

KW - Acid number

KW - Analysis chemistry

KW - Hexanitrohexaazaisowurtane

KW - Indicator

KW - Titration

UR - http://www.scopus.com/inward/record.url?scp=33846149309&partnerID=8YFLogxK

M3 - Article

AN - SCOPUS:33846149309

SN - 1006-9941

VL - 14

SP - 397

EP - 399

JO - Hanneng Cailiao/Chinese Journal of Energetic Materials

JF - Hanneng Cailiao/Chinese Journal of Energetic Materials

IS - 5

ER -

Determination of acid number in hexanitrohexaazaisowurtane by method of titration

摘要

其它文件与链接

指纹

引用此