Thermal safety study of bistetrazolohydrazine

Zhiyue Han; Tonghui Yang; Zhiming Du; Linshuang Zhao; Xiaomin Cong; Zerong Guo

doi:10.1016/j.proeng.2014.10.454

Thermal safety study of bistetrazolohydrazine

Zhiyue Han, Tonghui Yang, Zhiming Du^*, Linshuang Zhao, Xiaomin Cong, Zerong Guo

^*Corresponding author for this work

School of Mechatronical Engineering

Beijing Institute of Technology

Research output: Contribution to journal › Conference article › peer-review

1 Citation (Scopus)

Abstract

The thermal decomposition behavior of HBT was studied by TG-DSC thermal analysis method. The decomposition products of HBT were analyzed. TGA curves and differential thermal curves of HBT were measured in different heating rates. The activation energy and pre-exponential factor of HBT was separately calculated by Ozawa equation and Kissinger equation. Thermal decomposition Mechanism of HBT were derived by Ozawa equation and its possible mechanism function was got. The differential thermal curves of HBT prepared by different dispersants were measured and the kinetic parameters were obtained. These kinetic parameters are in good agreement. The test values of the HBT dispersed with acetone have a higher accuracy, so the activation energy calculated is more meaningful.

Original language	English
Pages (from-to)	436-448
Number of pages	13
Journal	Procedia Engineering
Volume	84
DOIs	https://doi.org/10.1016/j.proeng.2014.10.454
Publication status	Published - 2014
Event	2014 9th International Symposium on Safety Science and Technology, ISSST 2014 - Beijing, China Duration: 4 Nov 2014 → 6 Nov 2014

Keywords

Bistetrazolohydrazine
Nitrogen-rich compound
Thermal analysis

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10.1016/j.proeng.2014.10.454

Cite this

@article{1fa6e59fd4a243b1901fd2a0ba96441f,

title = "Thermal safety study of bistetrazolohydrazine",

abstract = "The thermal decomposition behavior of HBT was studied by TG-DSC thermal analysis method. The decomposition products of HBT were analyzed. TGA curves and differential thermal curves of HBT were measured in different heating rates. The activation energy and pre-exponential factor of HBT was separately calculated by Ozawa equation and Kissinger equation. Thermal decomposition Mechanism of HBT were derived by Ozawa equation and its possible mechanism function was got. The differential thermal curves of HBT prepared by different dispersants were measured and the kinetic parameters were obtained. These kinetic parameters are in good agreement. The test values of the HBT dispersed with acetone have a higher accuracy, so the activation energy calculated is more meaningful.",

keywords = "Bistetrazolohydrazine, Nitrogen-rich compound, Thermal analysis",

author = "Zhiyue Han and Tonghui Yang and Zhiming Du and Linshuang Zhao and Xiaomin Cong and Zerong Guo",

note = "Publisher Copyright: {\textcopyright} 2014 The Authors. Published by Elsevier Ltd.; 2014 9th International Symposium on Safety Science and Technology, ISSST 2014 ; Conference date: 04-11-2014 Through 06-11-2014",

year = "2014",

doi = "10.1016/j.proeng.2014.10.454",

language = "English",

volume = "84",

pages = "436--448",

journal = "Procedia Engineering",

issn = "1877-7058",

publisher = "Elsevier B.V.",

}

TY - JOUR

T1 - Thermal safety study of bistetrazolohydrazine

AU - Han, Zhiyue

AU - Yang, Tonghui

AU - Du, Zhiming

AU - Zhao, Linshuang

AU - Cong, Xiaomin

AU - Guo, Zerong

PY - 2014

Y1 - 2014

N2 - The thermal decomposition behavior of HBT was studied by TG-DSC thermal analysis method. The decomposition products of HBT were analyzed. TGA curves and differential thermal curves of HBT were measured in different heating rates. The activation energy and pre-exponential factor of HBT was separately calculated by Ozawa equation and Kissinger equation. Thermal decomposition Mechanism of HBT were derived by Ozawa equation and its possible mechanism function was got. The differential thermal curves of HBT prepared by different dispersants were measured and the kinetic parameters were obtained. These kinetic parameters are in good agreement. The test values of the HBT dispersed with acetone have a higher accuracy, so the activation energy calculated is more meaningful.

AB - The thermal decomposition behavior of HBT was studied by TG-DSC thermal analysis method. The decomposition products of HBT were analyzed. TGA curves and differential thermal curves of HBT were measured in different heating rates. The activation energy and pre-exponential factor of HBT was separately calculated by Ozawa equation and Kissinger equation. Thermal decomposition Mechanism of HBT were derived by Ozawa equation and its possible mechanism function was got. The differential thermal curves of HBT prepared by different dispersants were measured and the kinetic parameters were obtained. These kinetic parameters are in good agreement. The test values of the HBT dispersed with acetone have a higher accuracy, so the activation energy calculated is more meaningful.

KW - Bistetrazolohydrazine

KW - Nitrogen-rich compound

KW - Thermal analysis

UR - http://www.scopus.com/inward/record.url?scp=84922276532&partnerID=8YFLogxK

U2 - 10.1016/j.proeng.2014.10.454

DO - 10.1016/j.proeng.2014.10.454

M3 - Conference article

AN - SCOPUS:84922276532

SN - 1877-7058

VL - 84

SP - 436

EP - 448

JO - Procedia Engineering

JF - Procedia Engineering

T2 - 2014 9th International Symposium on Safety Science and Technology, ISSST 2014

Y2 - 4 November 2014 through 6 November 2014

ER -

Thermal safety study of bistetrazolohydrazine

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Keywords

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